GCMS calibration table for TCLP analysis, Dec 5 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Ethanol, 2-(2-ethoxyethoxy)-, Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.29 1.47 ng/uL 513104 1,4 -Diehlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2-2-ethoxyethoxy)-, aceta 176 C8H1604 000112-15-2 33 2 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 17 3 Oxirane, 2-butyl-3-methyl- , cis- 114 C7H140 056052-93-8 12 4 CH2=CHCHZC (O) OCH3 100 C5H802 003724-55-8 10 Abundance Scan 594 (10.292 min): 26712.D (-) m/ z 43.10 100.00% 43

5000

—— 1 57 73 85 LA 10.00 10.20 10.40 10.60 — 30 37 40 L 501 .. 70 80 90 100 110 100 120 130 m/z 57.10 30.54% miz-> 20 50 60 Abundance #16609: Ethanol, 2-(2-ethoxyethoxy), acetate 43

i 5000 31 59 ■ ■ n — LA 10.00 10.20 10.40 10.60 l 72 m/ z 59.10 30.11% -30....40 I—50 |, || 87 _ 103 , , , , —132 miz- 20 60 70 80 90 100 110 120 130 Abundance #1531: Oxirane, 2-methyl-3-propyl-. cis- 43 i 4 4 ■ 10.00 10.20 10.40 10.60 57 5000 71 85 m/ z 41.10 28.81%

I | 100 50 60 70 80 ' 90 100 110 120 ‘ 130 miz->20 30 40 'Abundance 43 #3063: Oxirane, 2-butyl-3-methyl-, cis- + , 1 4 s4 ss 10.00 10.20 10.40 10.60 m/ z 55.10 28.78% 55 5000- 85 71

1 h 1 1 I ' ' ' ' I1 1 ' I ' ' 1 99 114 A miz-> 20 30 40 50 60 70 80 90 100 110 120 130 10.00 10.20 10.40 10.60

26712.D NP112701.M Fri Dec 07 13:15:19 2001 Page 7

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