GCMS analysis results for sample AD26682, Dec 10 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26682.D vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 Hexane, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.29 1.56 ng/uL 536140 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 2-methyl- 100 C7H16 000591-76-4 38 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 35 3 Ethanol, 2- (2-ethoxyethoxy)- , aceta 176 C8H16O4 000112-15-2 33 4 Hexan- e, 2-methyl- 'Abundance 100 C7H16 000591-76-4 25 Scan 594 (10.291 min): 26682.D (-) m/z 43.10 100.00% 4

5000 57 85 ===...... — = — 4 73 440 514— ul 10.00 10.20 10.40 10.60 100 TIPTTTT m/z S'7-1.0 32.42% m/z-> 10 20 30 50 60 70 80 90 100 110 120 130 ’Abundance #63433:- Hexane, 2-methyl- i 43

5000 57 85 -----A- IL 10.00 10.20 10.40 10.60 m/z 59.1.0 31.66% ! 27 .1 1 1 1 T I 1 71 TTT _ 100 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 'Abundance #637: Pyrrolidine, 3-methyl- 43 —IPPIBT A 10.00 10.20 10.40 10.60 5000- m/z 41.10 30.33% 85 i

m/z-> Abundance — 15

10 27

20 ■ i ■ ' ■ ■ i • 30 40

43 50 I 60 70 56 80 68 ■ i ' ' ■ • i ■ ' ' ' i ' 1 1 1 i ' ' ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' ' ' ' i 90 100 110 #16609: Ethanol, 2-(2-ethoxyethoxy)-, acetate 120 130 4 4 । P—4 — 10.00 10.20 m/z 55.10 A 10.40 10.60 30.28% 5000 31 59 72

m/z-> । • i ■ ■ ■ ■ i' ■ ■ ■ i • ■ ■ ■ । ■ 10 20 30 40 I -- 50 60 70 87 103 ' ‘ I ' ' TTT . . . . I . . . . I . M . I . 80 90 100 110 120 132 130 -4 10.20 10.00 10.40 10.60

26682.D NP112701.M Fri Dec 07 13:13:30 2001 Page 10

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