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GCMS analysis results for sample AD26315, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26315 with unidentified compounds detected.

NYC-WTC_000031248–000031261

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26315.D vial: 24 Acq On 1 Dec 2001 9:07 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 5 2-Pentanol, 3-chloro-4-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.52 0.55 ng/uL 156106 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, 3- (R@ 136 C6H13C1O loro-4-methyl-, 074685-47-5 40 2 2-Hexanol / 102 C6H140 000626-93-7 38 3 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 4 2-Hexanol/ 3-methyl- 116 C7H160 002313-65-7 33 Abundance Scan 620 (10.524 min): 26315.D (-) m/z 43.05 100.00% 43

5000

57 85 4 A— • • I • ’ 1 * I 61 69 10.20 10.40 10.60 10.80 mH —JH m mmm TTTTp-rTTpT-TTpTTT-p-rrr m/z 45.10 76.53% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #6421: 2-Pentanol, 3-chloro-4-methyl-, (R@,R@)-(.+/-.)- 45 ......................... ......................

5000 10.20 10.40 10.60 10.80 m/z 41.10 32.18% 27 58 . _ 6976 85 100 TTTTTTT + H 1111111 [ 11 Tg r 1111 11 11 i111111 Tp 1111111111111111111111111111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583:2-Hexanol 45 A AAloAAk ‘IA a 10.20 10.40 10.60 10.80 5000 m/z 85.05 20.12%

27 39 69 55 - - mmHtpn > । ■ >. 111 >... ।. j... > ।87 , 1 > > ।.... ।.... ।.... (. miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 1’111 I • ■ ‘ * 1 1 10.20 10.40 10.60 10.80 —A m/z 57.10 17.52% 57 5000 71 85

m/z—> -l — mr +TTTTrr —001101/ — 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 A 10.20 10.40 10.60 10.80

26315.D NP112701.M Tue Dec 04 10:11:46 2001 Page 5

NYC-WTC_000031260

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NYC-WTC_000031260Source: NYC Law Department, mirrored locally

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