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GCMS analysis results for sample AD26828, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032182–000032201

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032200
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26828.D Vial: 12 Acq On 6 Dec 2001 8:12 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 2-Hexanol Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.52 0.79 ng/uL 196694 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 40 2 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 38 3 2-E Pentanol, 4-methyl- 102 C6H140 000108-11-2 36 4 27P entanol, 3-chloro-4-methyl- , (R@ 136 C6H13C1O 074685-47-5 36 Abundance Scan 620 (10.524 min): 26828.D (-) m/z 43.10 100.00% 43

5000

57 85 J ' ' I ' ' TT I ' TT

I miz-> ‘ I 20 25 TI" 30 m1 39 m—Ilm 61 69 35 40 45 50 55 60 65 70 75 ‘I‘ 80 85 90 95 100 105 10.20 10.40 10.60 10.80 m/ Z 4 5.10 84.87% Abundance #63583: 2-Hexanol 45

5000 — , , 1 . 111 1 ' I 10.20 10.40 10.60 10.80 m/ z 41.05 28.23%

m/z-> 20 ... 7731... 22—4... 25 30 35 40 55 45 50 55 60 65 70 75 80 85 87 90 95 100 105 'Abundance #1531: Oxirane, 2-methyl-3-prepyl-. cis- 43 -a------=n4 10.20 10.40 10.60 10.80 57 5000 71 85 m/ z 35.05 17.16%

100 I.... 1. 111 f. I.... I TT’ ‘I i • ■ ■ ■ i TTT’II’IIIF T1TTTNIT, m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-methyl- —— 45 10.20 10.40 10.60 10.80 m/ z 57.10 16.69% 5000

miz-> -mm 27 P 44 . . 4... 4487, 57

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 i'''' i'''' i .A A 10.20 10.40 10.60 10.80 ‘T

26828.D NP112701.M Fri Dec 07 14:53:37 2001 Page 11

NYC-WTC_000032200

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