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GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28171 analyzed on January 2, 2002.

NYC-WTC_000035365–000035380

Folder label: “GCMS X 11/26/01 A 12/22/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2 10128172.D Vial: 38 Acq On : 22 Dec 2001 2:53 pm Operator: GALOS Sample gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Hexanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.43 0.88 ng/uL 213085 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 38 2 2-Hexanol 102 C6H140 000626-93-7 38 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 37 4 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 Abundance L Scan 610 (10.434 min): 28172.D (-) m/z 43.10 100.00% i 43

m/z-> 5000

- + 16 T-q-r 39 • 20 25 30 35 40 45 50 1 53+44 55 57 61 69 85 --- 10.00 10.20 10.40 10.60 10.80 - - 11 " " I " 1 < TTTmt m/z 60 65 70 75 80 85 90 95 45.10 69.34% 1 Abundance #63583: 2-Hexanol 1 45

5000- TT * 10.00 10.20 10.40 10.60 10.80 27 I 31 39 42 55 58 69 | 84 87 m/ Z 41 • 10 27.93% 1 11 ■ '' • i' ■' 11 I ‘ ■ I ■ TTrr T ; H I I TCCTgr M I | I I I I | I I I I TTTr | । । । । | । 1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2-Hexanol 45 -A — -44—— — 10.00 10.20 10.40 10.60 10.80 5000- ■ m/ z 85.15 21.89%

l 27,3! 39 42 , 55 58 69 34 87 I TIPnTTmmTgr ‘ r ' ' 'l ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' TTTTT i I I i i | | | | i i r rr...... .. rn/z-> 20 25 30 35 40 45 50 55 . 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- A II 45 10.00 10.20 10.40 10.60 10.80 m/z 57 •10 17.02% 5000-

=- 69 27 42 57 ......... .......... TTTTTHTTT I 84 87 ' ' I ' ' ' ' I TTrtTn | ' in | r Trr \ II A m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10.00 10.20 10.40 10.60 10.80

28172.D NP112701.M Fri Dec 28 09:08:23 2001 Page 6

NYC-WTC_000035378

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NYC-WTC_000035378Source: NYC Law Department, mirrored locally

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