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GCMS analysis results for sample AD26829, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26829 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032202–000032222

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26829.D Vial: 6 Acq On 6 Dec 2001 2:44 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Pentanol, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.12 1.44 ng/uL 414360 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 36 2 1-Buta: nol 74 C4H10O 000071-36-3 33 3 Cyclop*ropane, (1-methylethyl )- 84 C6H12 003638-35-5 12 4 Cyclobutane 56 C4H8 000287-23-0 9 Abundance Scan 31 (5.123 min): 26829.D (-) m/z 41.05 100.00% 1

'm/z-> 5000

'Abundance 5 10 15 20 25 35 41

3& ■ ■ • ■ i • ■ ■ ■ I ■ ■ ■. 111111 • < ■ ■ i ■ • ■. i ■ > I 30 + 45 56 59

40 45 50 55 60 65 50 53 111

#63578: 1-Pentanol, 4-methyl- + 71 +. 67.70.75 80 85 90 ■ ■ i' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z N__ 75.01%

1 56 41 I 69 5000 — I'1'11' 1 4.90 5.00 5.10 5.20 5.30 5.40 5.50 I m/ Z 59.10 71.96% i 45 ' ’’TT’E77 | i r ■ ■ | i i 1 , [ । i t I | i । ' । | i r ' । | I 1 i ■1 ■ ■ i' I I 59 11 1 ■' 111 ■1 r ■ ‘' 1111' r 11 ' i' 84 m/: 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62584; 1 -Butanol 41 56 i' ■'' I V 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 43 .05 65.06%

i m/z-> Abundance 1 5 10 ...... 38+44 15 20 25 30 35 40 45 ' 11153’111'' 50 #592: Cyclopropane, (1-methylethyl)-

41 $ I 1111111 turrrr I I I 1 1 I I 1 1 I I I I I I I I 55 60 65 70 75 80 85 90

m/ z /W. 4.90 5.00 5.10 5.20 5.30 5.40 5.50 42.05 63.67% 5000- 27 69 15 37 ' r " ' i'''' i I. —50534 ,... 1.... ... 1 ■ ■ i'''' i'''11 ■ ■' ■ i'' ■ ■ 111'' i'''' r l' " 111 " TpT ral r, TTTIT . m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26829.D NP112701.M Fri Dec 07 14:54:25 2001 Page 2

NYC-WTC_000032210

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