GCMS analysis results for sample AD26829, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26829.D Vial: 6 Acq On 6 Dec 2001 2:44 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3,5-Hexadien-2-ol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.02 g/uL 319428 1,4-Dichlorobenzene-d4 11.89

Hit# of Tentative ID MW MolForm CAS# Qual

1 3,5-Hex. 2 -Ol 98 C6H10O 003280-51-1 40 2 1-Butan ethyl- 102 C6H140 000097-95-0 23 3 Isoxazo methyl- 83 C4H5NO 005765-44-6 9 4 2-Pentan 3-methylene- 98 C6H10O 004359-77-7 9 Abundance Scan 20 (5.022 min): 26829.D (-) m/z 43.0 100.00% 4

5000

39 51 — .........I"" 55

, 69 1..65.1. . 80— 1185 90 A100 83

98 _/W_ 4.90 5.00 5.10 5.20 5.30 5.40 m/z 55.10 44.80% I’

Jul m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 95 105 'Abundance #1271: 3,5-Hexadien-2-ol 43

5000 55 I '• ’* I ' ' ' • I ' '’ ‘ I ' '* ' I TT 83 4.90 5.00 5.10 5.20 5.30 5.40 79 98 m/z 83.05 41.36% 51 I 71 li mPPT I j .It mT • 111 ‘ I Tpf i111' m!z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63559: 1-Butanol. 2-cthyl- 43 .. L I 1 ‘ ‘ ’ I ' ' ’ ‘ I i ■ ■ • ■ i TT 4.90 5.00 5.10 5.20 5.30 5.40 5000- m/z 42.05 23.02% 27 31 . 55 70

N 84 ,59 '11'11111 ” ‘ I ’ n 1 r ■ " i " 111'1" 111IUICmpunuut m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #512: Isoxazole, 5-methyl- l ■ ■ ■ ■ i Trmrr T 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z 41.05 21.78% 83 5000- 68 ।i 27 39 54 IIdTTTH ' i' • " i1 - ■ i" " i ■ • ■ ■ ।11 • i" " r T’tr’i i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ । > ■ ■ • । । | i * • » । » m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40

26829.D NP112701.M Fri Dec 07 14:54:23 2001 Page 1

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