NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC0601\26828.D Vial: 12
Acq On 6 Dec 2001 8:12 pm Operator: ‘GALOS
Sample gc/ms unknown Inst : GC/MS Ins
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator)
Title : 208 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 1 3-Hexene-2,5-diol Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
5.00 1.29 ng/u 322166 1,4-Dichlorobenzene-d4 11.89
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
l 3-Hexene-2,5-diol 116 C6H1202 007319-23-5 45
2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 45
3 1,3 -Oxathiolane- 2-propanol, 2-methy 162 C7H14O2S 036651-30-6 36
4 1-Butano , 2-ethyl- . 102 C6H140 000097-95-0 23
Abundance 7 Scan 18 (5.004 min): 26828.D (-) m/z 43.00 100.00%
/W...
43
5000
55 83
; 39i| 69 ..................... 98 4.90 5.00 5.10 5.20 5.30 5.40
; - ---- 11" ' TI51 T ---HH m/z 55.10 22.60%
m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
It
Abundance #3285: 3-Hexene-2,5-diol
43
5000 I' ' ’ ■ I
4.90 5.00 5.10 5.20 5.30 5.40
55 83
m/z , 83.05 21.50%
98
61 71
Hmmmpp
i' ■ " i
m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
Abundance #1244; 4-Penten-2-one, 4-methyl-
i 43
I ■ ■ •' I
4.90 5.00 5.10 5.20 5.30 5.40
5000 m/z 42.00 13.89%
83
29 39 55 98
I I
' i " " I " '11" " i1 TTT ' i " " r • " r " ■ i " " i " " i ■ " • i " 1' i " ' ■ r ■ " i1111111 " 111
m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
Abundance #12808: 1,3-Oxathiolane-2-propanol, 2-methyl-
. ..
I’TE’TCCTTETTTTETTTETTTT
48 4.90 5.00 5.10 5.20 5.30 5.40
m/z 41.00 12.98%
| 84
5000-
54 go
m/z->
TTT’TT 11111 i! । TTTT 111111
20 25 30 35 40 45
TTTTT 1.60... 62.......
50 55 60 65 70 75 80 85 90 95 100 105
'r"'i""i""I" | TTY . । > i . . । Il....I.T I ! (I t n |
4.90 5.00 5.10 5.20 5.30 5.40
26828.D NP112701.M Fri Dec 07 14:53:17 2001 Page 1
NYC-WTC_000032190
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