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GCMS analysis results for sample AD26676, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031968–000031988

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031976
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26676.D Vial: 9 Acq On 6 Dec 2001 5:28 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L . ********************************************************************* Peak Number 1 5-Hexen-2-one Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.00 1.42 ng/uL 438200 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Hexen-2-one 98 C6H10O 000109-49-9 9 2 Pentane/ 2,3,4-trimethyl- 114 C8H18 000565-75-3 9 3 1,3 -Oxathiolane-2 -propanol, 2-methy 162 C7H14O2S1 036651-30-6 9 4 2-Pentanone, 5-hydroxy- 102 C5H10O2 001071-73-4 9 Abundance / Scan 18 (5.005 min): 26676.D (-) m/z 43.00 100.00% 43

5000 -

55 83 as 4.90 5.00 5.10 5.20 5.30 5.40 ' । — 341 49 , ------- 70 1 98 m/z , 55.10 14.22% m/z-> 20 30 40 50 60 70 80 __ 90 100 110 120 Abundance #1291: 5-Hexen-2-one I 43 i

5000- ।>.r>।.>..।.<>.।>..>। i ■ ■ • ■ i 4.90 5.00 5.10 5.20 5.30 5.40 55 m/z 83.05 13.36% 27■ ' I ' ' 37 50 | 69 83 98 ' ■ I i ■ ■ ■ • । » i • ‘ • i > ■ • • । ---------- m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3100: Pentane, 2.3.4-trimethyl- 43 I’I i • ■ ■ ■ i । • •• ■ । •• • • । 71 4.90 5.00 5.10 5.20 5.30 5.40 5000 - m/z 42.05 10.71% 55

A., I 27 114 . . 1 . . I I I . ... I .... I > ... 1 . • ■ i > > • • i ■ 1 ' ■ i ' ' miz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #12808: 1,3-Oxathiolane-2-propanol. 2-methyl- IrTur l .. . , I . ., . I,, , , TTTmrrr , T 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z 41.0,5 8.37%

jL 84 5000

54 so -......................... ! ,,, III 60I I I I 9 ' ' I ' ' ........ 1 ' ’ i » ' 1 ' I ' ’ ‘ ' J • • • » I • I I I I I I I I m/z-> 20 30 40 50 60 70 80 90 100 110 120 4.90 5.00 5.10 5.20 5.30 5.40 j

26676.D NP112701.M Fri Dec 07 14:51:22 2001 Page 1

NYC-WTC_000031976

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NYC-WTC_000031976Source: NYC Law Department, mirrored locally

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