GC/MS analysis results for sample AD30935, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.29 ug/1 77778 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 91 2 3,6-BiS (N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 25 3 2 (1H) -Pyrimidinone, 5-chloro-4,6-di 282 C16H11C1N2O 028567-83-1 9 4 2-Oxo-4-phenyl-^(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 Abundance ’ Scan 663 (11.128 min): 30935.D (-) m/z 281.00 100.00% i 201

5000

■ ■ i ■ ■ ■ 1 1 ■ ■ ■ ■ ITTT’1 > । 1 । । 35 49 73 86 103 119 133 163 177 123 207 249 265 | 10.80 11.00 11.20 11.40 I, L ill m/z 282.00 31.32% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 {Abundance #41966; Cyclotetrasiloxane, octamethyl- I 281

5000 10.80 1100 11.20 11.40 ' m/z 283.00 17.21% 133 73 | 163 177 191 207 235 249 265 | VQ-if-r i j i i . । । । । ■ । । । <« t । । । > । । > • i i j । । i ’ i ’ 4 jI • r' • 11»1 111 ■"'! । । Ai 11 |" । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3.6-Bis(N-dimethylamino)-9-ethylcarbazole 281 * * i * • * * i • * • > i * * * * । > > * ' । 10.80 11.00 11.20 11.40 5000 m/z 192.90 11.26% 266 141 208 222 237 250 m/z-> 40 60 80 100 120 140 160 180 266' 220 240 260 280 Abundance #39758:2(1H)-Pyrimidinone, 5-chloro-4,6-diphenyl- r r I * ’ • ‘ I 1 1 1 * I’’’’ I I I I I J J I' 281 10.80 11.00 11.20 11.40 m/z 132.90 10.52% 5000 77 104 247 ■ ■ i ■ ■ ■ ■ i.. .i'i . ■ ■. r ................ 204...... 1...... ’*1****I’*’*I+*’*l’ ’’1’***I****1+’’’1++’II ' ‘ I ‘ • I ‘ ‘ ' 1 I 1 1 1 r| । 1 1 । | miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30935.D GCMS1126.M Fri Jan 25 11:50:20 2002 Page 2

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