Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
NYC-WTC_000018754–000018774Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration’ Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.30 1.75 ug/1 569671 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, oamethyl- 370 C10H3005Si5 000541-02-6 64 2 N-(Trifluoroacetyl)N, 0,0',O'•-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 N-(Trifluoroacet )-0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 4 3,4-Dihydroxyben yl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 Abundance Scan 1009 (14.305 min): 30935.D (-) m/ z 73.0.0 100.00% 73
5000 267 355 i 45 14.00 14.20 14.40 14.60 — . •99 125 154 J 223 1 .193 223 293 323 j-1 * ■ • 144.1 r । . r. V I 1 / < । .i । . . m/z " 33.28% miz-s 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- I 73 355 267 • > * l ■ > ■ 1 I > 4 i >t 5000 T 14,00 14.20 14.40 14.60 m/z 355.05 24.43%
miz-> 17r l 50 -7 100 150 200 250 ■ 323. i i
300 350 ■ r • ■ ■ ■
400 i ■ • ■ ■
450 i • ■ ■ •
500 i ■ ■ ■ ■
550 i ■ ■
Abundance #60162; N-(T riflueroacetyl )-N O. O', O"-tetrakistrimethylsi 73 . ......4 355 14.00 14.20 14.40 14.60 | 5000 m/z 267.90 8.62%
45 t 147 193 267 538 1 ' t ’ ■ ■ ■ i 1 ' ‘ • i ' ‘ ' i 1 '' 1 1 I 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 (Abundance #58326: N-(Trifluoroacetyl)-O,O',O”-tris(trimethylsilyl)no 73 14.00 14.20 14.40 14.60 ‘ 355 m/z 356.05 8.45% 5000
45 I 120147 193 265 481 miz-> 50 100 Ta—nnnmmTTTTTTATIT 150 200 ■ * • i • • • • i . • 250 300 350 400 450 500 550 T T• l *.. . 14.00 14.20 14.40 14.60
30935.D GCMS1126.M Fri Jan 25 11:50:25 2002 Page 3
NYC-WTC_000018763
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
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NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
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