Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
NYC-WTC_000018248–000018261Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On : 2 Jan 2002 12:47 am Operator: 209 GALOS Sample : gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********** *** ************************************* ** ***************** Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
11.12 1.99 ug/1 572193 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetri iloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 Benzenel-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 2-Oxo-4 -phenyl-6-(4-chlorophenyl) -1 282 C16H11C1N20 000000-00-0 7 4 6,7 enzo-phenothiazine-5,5-dioxide 281 C16H11N02S 000000-00-0 5 Abundance Scan 662 (11.125 mln): 30984.D (-) m/z 281.00 100.00% 201
5000
73 45 59 . . । i' -. | 89 103 119 ‘33f147 , । v । ,163 rt f >. r, i । t . ) "I r, / I?» j177 123207 "T"I i "T" 221 235 2^. 265 rr m/z 11"I IITIINMTIIB4II 10.80 11.00 11.20 11.40 282.00 30.32% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.80 11.00 11.20 11.40 73 133 . 207 m/z 283.00 18.95% .......... 73 ............... 1...... 163 177 191 L 235 249 265 | n* 1 ‘ 1 I 1 tt i | i’i i i fi i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene. 1 -pheny/-4-(2-cyano-2-phenylether VI) 281 >■> । > । । । । > • 1 i ■ ■ 1 ■ i 10.80 11.00 11.20 11.40 5000 m/z 133.00 12.09% 126 203 i 224 240 ■ ■ । ■ ■ ■ ■ । ■ • ■ ■ । ■ • ■ ■ । ■' ■ ■ ।' ’ । r i ’ » j . ‘C1 . . ri j...।।ijii।i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl}-1,2-dihydropyrimi 281 10.80 11.00 11.20 11.40 m/z 192.90 12.07% 5000
102 123 141 175 204 247 || ■ ‘ i ■ ■ ' ‘ i • ■ 1 • i • ■ ■ • l 1 ■ i •1 ■ ■ i • 1 I 1 1 1 ' I 1 1 1 1 11 1 ' 1 "11 1 1 r I 1 1 11 1 1 ' I'' m/z-> 40 60 80__ 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30984.D GCMS1126.M Wed Jan 23 08:53:24 2002 Page 2
NYC-WTC_000018256
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder