GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\ JANO 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

18.01 0.51 ug/1 171766 Acenaphthene-dl0 20.39

Hit# of 5 Tentative ID MW MolForm CAS# Qual

12-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 32 2 2 (5H) -Furanone, 3,5,5-trimethyl- 126 C7H10O2 050598-50-0 17 3 Butane / 58 C4H10 000106-97-8 10 4 3-Penten-2-one, 4-methyl-, o-methyl 127 C7H13NO 056336-11-9 9 Abundance 43 Scan 1412 (18.009 min): 27288.D (-) m/z 43.00 1 00.00% 57 73 5000 111 95 ■p=r W 17.60 17.80 18.00 18.20 18.40

miz-> • • i ■ ■ ■ • i ■ ■ *11' 10 20 30 36, 1 lk 50,1 40 50 60 70 80 90 85 ■ i ■ I’t’i I'111111, ■ ■ । • ■127 ..11 .I di 100 110 120 146 ’ , >, 11, ‘ l " 130 140 150 m/ z 57.00 60.65% Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43

5000 17.60 17.80 18.00 18.20 18.40 27 58 73 m/z 73.00 51.97% | i. I ■ ■ i ■ ■ ■ • i ■ ■ • ■ i ■ 7 111 1111 i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■1 ■ i ■ ■ ■ ■ i •1 ■ ■ i ■' • ■ i • ■ ‘ • i ■ • ■ ■ i • ■ ‘ ■ i • ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance 4147 25 -F ■ #am0r imee 43

17.60 17.80 18.00 18.20 18.40 5000 111 m/z 111.10 41.31% 83 55 126 68 ‘ ■ i ■ ■1 ■ i11 ■ • i ■ ■ ■ • i ■ • ■ ■ i • ■ ■ ■ i ■ ■ ■11 ■ ■1 • i1 ■ i ■ ■ ‘ ■ i ■' ■ ■ i1 ‘ ‘ ‘ i i ’“ i ■1" i “ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #99: Butane 43 17.60 17.80 18.00 18.20 18.40 m/z 69.10 24.93% 5000 29

15 58

miz-> H noiis] 1'11 ■ ■

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 i' “ ' 1111' 111 ■ ■ i ■ ■ ■ ‘ i ■11 ‘ i'1' ■ i' ■ ‘' i •'' • i ■ • ■ ■ i ■ ‘ ........... 9,............. 17.60 17.80 18.00 18.20 18.40

27288.D GCMS1126.M Mon Feb 04 15:23:08 2002 Page 5

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