Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
NYC-WTC_000018005–000018025Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-1sopropoxy-1,1,1,7,7,7-hexam Concentrat ion Rank 3
R.T. EstConc Area Relative to ISTD R.T.
20.13 2.89 ug/1 969150 Acenaphthene-dl0 20.39
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1/T,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Trisiloxane, 1/1, 1,5,5,5 -hexamethyl 384 C12H3604S15 003555-47-3 42 3 4-Amino-5-imi dazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 10 4 Octadecanoic acid, 2-[(trimethylsil 386 C22H4603S1 056196-58-8 9 Abundance Scan 1643 (20.130 min): 27288.D (-) m/ z 73.00 100.00% 73
5000 147 281 327 19.80 20.00 20'20‘ 20.40111 45 117 to 191 । ■—221■ 2*5 249 1 355 383 415 - > > r - Fi "fr Pirin CATEB614* .. t ‘ ‘ 1 ■ । • ■ ■ ‘ । • ■ ■ ■ i ■ ' t al m/z 146.95 37.61% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isoprapoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 . . । . . । > । । r। . । 147 19.80 20.00 20.20 20.40 221 281 m/z 281.00 35.75% 111P-11TTT • i • • * ■ i • 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1.1,1,5.5.5-bexamethy3.3-bisi(trimet 73 147 ) i. 1 ’ • I ‘ r *l 1**1-I**4‘I 281 19,80 20.00 20.20 20.40 5000 m/z 326.90 14.31% 369 207 249, | 338 | miz-> 50 100 150 200 ' 250 300 350 400 450 500 ‘ 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 19.80 20.00 20.20 20.40 m/z 282.00 10.61% 327 5000
m/z—> 45 .. 147172 212, L 237
1 1508 *’I****1’’’I’*-1**’ ------- ' 550 ' 50 100 150 200 250 300 350 400 450 500 ....a.... 19.80 20.00 20.20 20.40 1
27288.D GCMS0103.M Thu Jan 10 09:36:54 2002 Page 5
NYC-WTC_000018017
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NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017980
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
Filed in the same folder
NYC-WTC_000017989
Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
Filed in the same folder
NYC-WTC_000017997
Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.
Filed in the same folder
NYC-WTC_000018026
Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
Filed in the same folder