Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 9.00 ug/1 4933580 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 2H-1,4-Benzoi .azepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 1,1,1,5,7,7, Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Silane, [1,2 -benzenetriyltris(oxy 342 C15H30O3Si3 __ 017864-23-2 12 Abundance Scan 1351 (17.450 min): 30707.D (-) m/ z 73.00 100.00%| 73
5000 341 147 429 45 17.20 17.40 17.60 17.80 , 96 117 [ 179.207225 251 281 311 L | 0-TI—E—mEumaampaaDTmr ..... 397........ L TTTpTTTpvrrp-rrrp- m/z 341.00 31.94% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 TBT 17.20 17.40 17.60 17.80 147 | m/z 147.00 15.03% ............. ,......... 117.... |............ 207 267 311 | jl j m/z-> 40 60 80 W0120140160180200 220 240 260 280 300 320 340 360 380400 420 Abundance 7 H i-Benzcdlazopin-2-pne 7-0 3-dihvdro-5 73 341 ................. 7 k...................... 17.20 17.40 17.60 17.80 5000 m/z 342.00 10.84% 45 1 91 J i 116 146 227 269 315, 11'11'1 “ I '' r ■ ‘ 'i ■" 'i" " i' ‘" I" "r' "r'" r •" i" ■ ■ r1 ■' r ■' ■ r1" r i' 'iH" i" " I" " 11"1111" 11 m/z->_____ 40 60 80 100120140160180200220240260280300320 340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 17.20 17.40 17.60 17.80 m/z 325.00 10.83% 147 5000- 267 355 429 45 207 ■'"i" "i"1'I" "I" "I" 1 .. .. .... 1... . 1'' I'i" " I ‘1" i" " i ■ I k I 1 1 1 1 i m/z-> 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30707.D GCMS1126.M Mon Jan 28 11:23:57 2002 Page 4
NYC-WTC_000004446
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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