Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.31 3.83 ug/1 2102740 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasil ane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzoic acid,./2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 3 3,4-Dihydroxy'benzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 4 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1009 (14.310 min): 30707.D (-) m/ z 73.00 1 00.00% 73 i 5000- 267 355 45 14.00 14.20 14.40 14.60 ___ i 133 154 177 193 , 223 251 |, IIITNITTT 89 108iTITTTuuPgu 293 323339 | ■' r ■ TI‘‘‘11‘1111 m/z 267.00 37.06% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- I 73 355 267 5000- 14.00 14.20 14.40 14.60 m/z 355.05 29.24% 191207 251 |, 323339 | 1Iu—nn)——uuunuouunmo ——mmpmmI"n0——tuur1Iu*unuaWnnanm m/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 451296: Benzoic acid 2,6-bisi(trimetbyisilyloxy]- trimet 73 355
14.00 14.20 14.40 14.60 5000- m/z 356.05 10.54% 147 267 249 47 208 ■ ■ i • ■ " i' " 11 ■ ■111 ” ■ ■ i ■ ■ ” i •1" i “ * ■ i1" ’ r1111 ■11 ‘ i *1111 +283 ' 11 • " I " " I ‘'1' i370 '"■i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- 73 14.00 14.20 14.40 14.60 m/z 267.90 9.64% 267 5000- 179 356 45 147 I . I, TP ‘111111 '' i ‘" i' " ' i1 ■ " i " '' i'1" i' ■ ■' i ‘ 209 237 312 341 ‘111111111111111111117111161101T l, m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30707.D GCMS1126.M Mon Jan 28 11:23:53 2002 Page 3
NYC-WTC_000004445
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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