Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.46 ug/1 199646 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 000556-67-2 72 296 C8H2404Si4 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 3,6-Bis (N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 40 4 4-Amino-5- /4- acetylphenyl azo) benzof 281 C14H11N502 000000-00-0 25 Abundance nd Scan 663 (11.134 min): 30707.D (-) m/z 281.00 ’ 100.00% 201
5000
45 59 73 89 103 119 133 147 163 177 123 207 221 235 249 265 10.80 11.00 11.20 11.40 TTTT ' ' ITuI, 1 1 * i" / । । . 7 i i i"| . i" । i"l । । । i < . । । < I « । ,, . ■ । r m/z 282.00 28.09% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260. 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281
5000 TIT I ' ' ■ । ■ ■ ■ ' । 10.80 11.00 11.20 11.40 265 m/z 283.00 16.15% 45 59 73 133 177 193 207 235 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 (Abundance +39643: Benzene 1 phenyi-4-(2-cyano-2-phenylethenvi) 281
10.80 11.00 11.20 11.40 5000 m/z 133.00 11.43% onn 253 126 203 266 224 240 , m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 281 10.80 11.00 11.20 11.40 i m/z 192.90 11.12% I 5000 266
141 208 222 2372“ - m1-00090mP-—m9m100m2md———m/ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30707.D GCMS1126.M Mon Jan 28 11:23:48 2002 Page 2
NYC-WTC_000004444
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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