Gas chromatography-mass spectrometry analysis of environmental sample AD26202 conducted Dec 5, 2001, identifying unknown compounds.
NYC-WTC_000031088–000031103Folder label: “GCMS X 11/2/01 A 12/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC0401\26202.D Vial: 71 Acq On 4 Dec 2001 1:21 pm Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.48 0.71 ug/1 230192 Naphthalene-d8 15.31
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606S16 000540-97-6 34 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 16 3 Silane, [1,2, /-benzenetriyltris(oxy 342 C15H30O3S13 017864-23-2 14 4 2H-1,4-Benzod iazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 14 Abundance / Scan 1354 (17.477 min): 26202.D (-) m/z 73.00 100.00% 73
5000 341
147 429 45 117 [ 179.207 251 17.20 17.40 17.60 17.80 L 295 111111171 TTTTTTTTTTTT mmmpk m/z 341.00 39.40% mlz-> 40 60 80 1001201401601802002202402602803003203403^)380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
5000 429 - +.. — 17.20 17.40 17.60 17.80 147 m/z 147.00 17.47% I 117. |..... ........... . I mz-> 40 60 80 100 120 140 160 180 200 220 240 260280 300 320 340360 380 400 420 ‘IT Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 17.20 17.40 17.60 17.80 267 rn/z 342.00 12.91% 5000 355 429 207
mlz-> L. _ Tung I ’111111110011—1011—01307711 T 40 60 80 100120140160180200220240260280300320340360380400420 TTp Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- IIP ' ' 1 I 1 PPI ' 73 239 17.20 17.40 17.60 17.80 m/z 324.90 12.04% 342 5000
45 133 '‘‘i" "I ........I,........211.. .mmmpmmmlmmmm IUI—ETIEEu"EI—U1—E0"11’7111 111111' 11 ■ • i • • • • । — m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
26202.D NP112601.M Tue Dec 04 16:05:44 2001 Page 5
NYC-WTC_000031100
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000031063
Laboratory report documenting GCMS analysis of sample AD26164 performed on December 3, 2001, noting other unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031171
Laboratory report documenting GCMS analysis of sample AD26206 with unidentified compounds detected.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030980
Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031003
Laboratory report documenting GCMS analysis of sample AD26131 conducted on December 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068413
Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068037
Laboratory report documenting GCMS analysis of sample AD24219 conducted on November 6, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068460
Laboratory report documenting GCMS analysis of sample AD24474 conducted on November 9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068748
Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069215
Laboratory report documenting GCMS analysis of sample AD25038 conducted on November 19, 2001, noting violations and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089203
Laboratory record for sample AD23719 showing detection of unknown compounds on October 17, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069644
Laboratory report documenting GCMS analysis of sample AD25460 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000030966
Single-page GCMS document identifier from the Environmental Protection Department archive covering late 2001 testing records.
Filed in the same folder
NYC-WTC_000030967
Administrative record of GCIMS scanning operations for World Trade Center environmental samples between November and December 2001.
Filed in the same folder
NYC-WTC_000030969
Laboratory report documenting GCMS analysis of sample AD26129 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030980
Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030992
Laboratory report documenting GCMS analysis of sample AD26130 conducted on December 3, 2001.
Filed in the same folder