Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D . Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 4.91 ug/1 2466980 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasi •xane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic acid , 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 N-(Trifl iroacetyl)-0,0',0’'-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Palmiti acid, 2-(trimethylsiloxy)e 372 C21H44O3Si 022613-62-3 35 Abundance / Scan 1009 (14.308 min): 30645.D (-) m/z 73.0,0 100.00% 73
5000 267 355 1 11 | । । । । | ri it | i i i ,
45 223 . L 293 323. i 14.00 14.20 14.40 14.60 i" I I ft T,193 108 133154 - 1 1703 Ft’T +*/1a/ i . । . *4, 1 m/z 267.00 35.94% /z- 50 Abundance 100 150 200 250 300 350 #51266: Cyclopentasiloxane, decamethyl- 400 450 73 355 267 5000 ■ ■ ।1 ■ ■ ■ i • • ■ ’ । • i • ‘ •11 14.00 14.20 14.40 14.60 m/z 355.05 27.54%
miz-> • ■ । 50 ........... 207 100 150 200 -23+ 250 300 350 400 450 Abundance #73978: Benzoic acid, 2.5-bis(trimethysiloxy)-, trimethyls 73 el 355 . Y .... . r । 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.89% 45 1 .If 179 223, 267 2972, ,............. miz-> Abundance 50 ‘ ' 100 ‘ ' 150 73 200 250 300 350 400 450 #58326: N-(Trifluoroacety!)-O,O‘,0"-tris(trimethyisilyl)no m 14.00 14.20 14.40 14.60 355 m/z 268.00 8.99% 5000
45 | 126147 193 265 376 481 • • i 1 • ■ ■ i ■ ‘ • 1 i • • • • I • ‘ ■ ■ i ■' • i • ' ■ • i 1 •'1 ■ i 1 ■ miz-> 50 100 150 200 250 300 350 400 450 14.00 14.20 14.40 14.60
30645.D GCMS1126.M Fri Feb 01 10:52:42 2002 Page 4
NYC-WTC_000018478
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder