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GCMS analysis results for sample AE02647, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02647.

NYC-WTC_000005448–000005462

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005459
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR0702\2647.D Vial: 20 Acq On : 8 Mar 2002 8:25 am Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.66 0.21 ug/1 36745 Acenaphthene-dl0 21.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid -ethoxy-, ethyl este 194 C11H1403 023676-09-7 95 2 Ethylparaben 166 C9H10O3 000120-47-8 49 3 Ethanone, 1-(4-ethoxyphenyl)- 164 C10H12O2 001676-63-7 45 4 1-Cyclopentene-1-propanoic acid, .b 168 C1OH1602 061833-30-5 42 Abundance Scan 1810 (21.658 min): 2647.D (-) । m/z 120.95 100.00% 121

149 5000 194 138 65 93 166 ........................ .... 21.40 21.60 21.80 22.00 80 | I ------------ 111" m/z 149.00 54.04% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 138 21.40 21.60 21.80 22.00 194 65 93 166 m/z 194.05 36.62%! 27 - ‘ I’’’ > I < I > > I > 1' I'' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance • . 121

21.40 21.60 21.80 22.00 5000 m/z 138.05 28.13% 65 93 138 166 53 TIWTUTgUTTUTTTTTTTETTTTTETITTTITTTTTTTIWTTTTTTTTWTTITT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #13415: Ethanone, 1-(4-ethoxyphenylj- ..... I ' ' I ' ’ ' 1 I ' 121 21.40 21.60 21.80 22.00

149 m/z 64.95 19.81% 5000 93 164 65

m/z-> 27 77 4 - '" 1,1,1" 11107 ' I " 111" " 1111' 111111r " ' I " '11‘WmmTp " 111" I " " I ‘ " 11' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 21.40 21.60 21.80 22.00

2647.D GCMS0208.M Wed Mar 13 14:58:31 2002 Page 5

NYC-WTC_000005459

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NYC-WTC_000005459Source: NYC Law Department, mirrored locally

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