GCMS analysis report for sample AE07001, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2402\7001.D Vial: 6 Acq On : 24 Apr 2002 8:41 pm Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.12 10.04 ug/1 996007 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual ?_________________ 1 Decanedioio acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 76 2 [1,1 ' -Biphenyl] -4-ol, 3-amino- 185 C12H11NO 001134-36-7 38 3 2,4,6(1H,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 25 4 Pyridine,/ 4 -[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 Abundance I Scan 3385 (36.123 min): 7001 .D (-) m/z 185.10 100.00% 185

5000 57 70 112 1 । | it Iu bOon । । T I । I । । । । 83 98 35.80 36.00 36.20 36.40 TT" —T | 125 143 166 . tt, al,1 r 4 Jr , 203 255268 282 297 315 m/ z 57.00 45.80% 1 ' 1 1 1 1 1 ' I 1 1 ■ ' I ' 1 1 1 I m/z-> 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000- 57 T 71 112 35.80 36.00 36.20 36.40 m/ Z 70.10 33.11% 98 —PH 125 143 166 203 '""'I'1......... 1 1 i ' 1 298 316 TII i' 1 1 1 i ’ ■ i ■ ■ 1 i' ' '

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #19199: [1,1‘-Biphenyl]-4-ol, 3-amino- 185 1 I | I I i I | I I i 1 [ I 1 I Td I । 1 [

35.80 36.00 36.20 36.40 5000 m/z 71.10 31.63%

139 156 113 7 I [ I I I i | i r I i | i I I I | I I i I | I I I I I I I r I 1 I I I I I 1 I I I I I I I I I I I I I I 11**’’|IIIII

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #31909: 2,4,6(1 H,3H,5H)-Pyrimidinetrione, 5,5-diethyl-1-(1- IIIIIIII**II’’S[II r r । 185 35.80 36.00 36.20 36.40 m/z 55.00 27.80%

5000- 211 70 54 96 ... | | 114 140155168 । | 225 240 T 1 | I I I I j I / ! , m - . 1 ' I -n-p-r-T-T-j-T-r — i । ii । i ] i । I ! । । । । । | । । । । । । । n । ii । i । r ।_ 11,n m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.80 36.00 36.20 36.40

7001.D GCMS0412.M Thu Apr 25 11:15:23 2002 Page 2

NYC-WTC_000043360