GC/MS analysis results for sample AD23651, Oct 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23651.D Vial: 5 Acq On : 15 Oct 2001 4:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Decanedioic acid, bis(2-ethylh Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 35.66 1.64 ug/1 235934 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual X^Decanedioic acid, bis (2-ethylhexyl) 426 C26H50O4 000122-62-3 87 2 [1,1'-Biphenyl]-4-01, 3-amino- 185 C12H11NO 001134-36-7 32 3 Butyl citrate 360'C18H32O7 000077-94-1 32 4 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 Abundance Scan 3336 (35.664 min): 23651 .D (-) m/z 185.10 100.00% Ite

5000 57 70 43 112

TTfe-> Abundance 40 60 ux 80 125139 166 203 297 315 ' I '' ‘ ' I ' ' '' I'' '' I' ' '' I' ' '' I' ' ' ' I' '' ‘ I'' ' ' I ' ' '' I '' '' I' 100 120 140 160 180 200 220 240 260 280 300 320 #55661: Decanedioic acid, bis(2-ethylhexyl) ester m/z 35.40 35.60 35.80 36.00 57.00 . 50.20%

Ite

5000 57 71 112 35.40 35.60 35.80 36.00 V Il 125 143 166 m/z 70.00 37.25% 203 298 316 A j I I I I ji rri j i iTi I I I I I I I I I I I I I I ' I ■ ' r ''' r ''' I''' I'''' I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260.280 300 320 i\bundance #19199; [1.1 '-Biphenyl]-4-ol, 3-amino- ----------------------- ,--- -1 As----------

35.40 35.60 35.80 36.00 253 m/z 71.00 34.49% A 156 139

I ' '' ' I ' ' ' ' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 <\bundance _ #50331: Butyl citrate_ ___________________ - .................. . - -.185------------------------------- -------35:40-.-35.60 35.80-36.00;" 129 Wz -112 TTO—Bl-T^ 5000

57 259 111 I I ■p-r+T 143^®^ I ''' ' I' ' '' I " ' • I 213 I'''' I I''' ' I'' '' I '' I I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.40.35.60 35.80 36.00

23651.D NP091101.M Wed Oct 17 10:05:20 2001 Page 4

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