GCMS analysis results for sample AD29790, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29790 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037146–000037155

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\DEC1401\29790.D Vial: 24 Acq On : 16 Dec 2001 12:56 am Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.57 0.49 ug/1 84765 Perylene-dl2 37.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 27 2 Nonane, 4methyl- 5-propyl- 184 C13H28 062185-55-1 17 3 Benzene,/l-nitro-2-(octyloxy)- 251 C14H21NO3 037682-29-4 12 4 2-Undecene, 2,5-dimethyl- 182 C13H26 049622-16-4 12 ‘Abundance ’ “ Scan 3325 (35.571 min): 29790.D (-) m/z 185.10 100.00% 185 57 5000 43 70 ! i 83 98 112

1 125 143 158 281 4- 35.20 35.40 35.60 35.80 36.00 l ...... — 1ir , > utl 1 ill il l •11'•■।' ■ ■ ■ । il li 208 । ■ ■ ■ ■ ।1 1-n-n-n-. ; ■ t i TIBBIII—r m/z 57.00 63.83% im/z-> 20 40 60 80__ 100 120 140 160 180 200 220 240 260 280 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

MAAA 44 A 5000 83 112 35.20 35.40 35.60 35.80 36.001 m/z 70.00 44.56% 42 ......... — 1. 98 | 199 217 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #19021: Nonane. 4-methyl-5-propyl- 43 57 71 AAA MA 35.20 35.40 35.60 35.80 36.00 5000 m/ Z 71.00 42.08% 112 27 85 I; I 127 141 184 | • ■ ■ < | ' ■ ■ ' | ■ 1 ' > | I 1 1 ' | ■ I 1 ■ | । । । । | । 1 1 • | ■ । । ‘ | • • ‘ 1 | ' । । ' | । ■ । ' | । । ' ‘ | > ■ ■ ■ | ■ ■

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 /, ! A Al A,

o Abundance #34102: Benzene, 1-nitro-2-(octyloxy)- A' I..... ' ' '' I ' ' 57 35.20 35.40 35.60 35.80 36.00 m/z 55.00 40.07% 71 5000- 83 112 139

m/z-> I ' ' ■ ' I ' ' 20 40 60 80 97 i 1 100 120 140 ..... ................. 221..... 251 ..... 160 180 200 220 240 260 280 wlpeAAqaM 35.20 35.40 35.60 35.80 36.001

29790.D GCMS1126.M Fri Dec 28 13:25:54 2001 Page 2

NYC-WTC_000037154

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GCMS analysis results for sample AD29788, Jan 2002 · Box DEP Box 22

NYC-WTC_000037156

Laboratory report documenting GCMS analysis of sample AD29788 conducted on January 9, 2002, by the DEP.

1 shared topics · Same agency, volume and box · similarity 0.999