GCMS analysis results, sample AD27953, January 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27953.D Vial: 9 Acq On : 20 Dec 2001 11:27 pm Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propanedioic acid, hexyl-, die Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.69 1.75 ng/uL 522715 Perylene-dl2 37.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 35 2 2-Undecene, /4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 25 3 Benzene, 1-nitro-2- (octyloxy) - 251 C14H21NO3 037682-29-4 23 4 2-Pyrimidinamine, 4-methyl-6-phenyl 185 C11H11N3 015755-15-4 22 Abundance Scan 3364 (35.687 min : 27953.D (-) m/z 185.10 100.00% 135 57

5000 71 43 112 83 98

; —L T’T ' ■ I 1 ■ ■ ■ i ' ■ i ' ' 125 143 158 203 35.40 35.60 35.80 36.00 281 297 + r i1. . r 4 TPP m/z 57.10 72.46% miz->____ 40___ 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 * Tr l_TTTTTT 83 112 35.40 35.60 35.80 36.00 42 m/z 71.15 46.77%

.1 j 981 , 1 ;............................. 199,217................... m/z—> 40 60 T-p-TTT-p-T —T 80 100 120 140 160 180 200 220 240 260 280 300 (Abundance #18485: 2-ndecene, 4,5-dimethyl-, [[email protected]@-(Z)]- 43 57 69 1 35.40 35.60 35.80 36.00 5000 m/z 70. ,5 46.34% j 83 98 112 140 I T-p-r-r-r-p-r ......... !_________ 182__________________________ ‘I‘‘‘111‘‘1111111111111111111I101IITIIITTITT 1 1 i 1 1 1 1 i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 (Abundance #34102: Benzene, 1-nitro-2-(octyloxy)- - ■ " | ■ 57 35.40 35.60 35.80 36.00 m/z 55.10 40.94% 71 5000 - 83 112 139

■ ■ i ■ ■ i1 b ■ ■ i 97 ! —...................... 221...... 251 .......... J y~

miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 35.40 35.60 35.80 36.00

27953.D NP112701.M Fri Dec 21 09:58:53 2001 Page 1

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