GCMS analysis results for sample AD27775, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27775.D Vial: 24 Acq On : 21 Dec 2001 4:56 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.68 1.42 ng/uL 361589 Perylene-dl2 37.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H24O4 005398-10-7 38 2 5-Undecene, 3-m< yl-. (Z) - 168 C12H24 074630-64-1 14 3 2-Undecene, 9-methyl- , (E) - 168 C12H24 074630-46-9 14 4 2-Undecene, 9-methyl -, (Z) - 168 C12H24 __ 074630-45-8 14 Abundance Scan 3363 (35.679 min): 27775.D (-) m/z 185.10 100.00% 57 185

70 5000 43 112 83 98 TTf............ —l , J., 1 ,1 _ 25, 103 158, . ■ ' i ' ' ■ ' i 203 35.40 35.60 35.80 36.00 i I‘" — ........... —281 m/z 57.15 80.70% miz-2 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32687; Propanedioic acid, hexyl-, diethyl ester _ rP 57 70

5000 83 112 35.40 35.60 35.80 36.00___ m/z 70.15 54.29% 42 : i 11 I I I < I I I I . i ■ ■ ■ ■ i 98 L...... 199 217....... miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #14794: 5-Undecene, 3-methryl, (2)- 55 70 ■ ■ i ■ ■ ■ ■ । ■ ■ i • ■ 35.40 35.60 35.80 36.00 5000 : 83 m/z 71.15 53.64% I

27 42 97 139 168 11 11111 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #14731: 2-Undecene, 9-methyl-, (E)- ■ ■ i p ■ ’ i ■ ■ 56 70 35.40 35.60 35.80 36.00 m/z 43.10 47.53% 83 5000

97 27 42 1 I ' ’1 ' I 11 II"T L... 139 , 168............ miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 35.40 35.60 35.80 36.00

27775.D NP112701.M Fri Dec 28 09:29:56 2001 Page 2

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