GCMS analysis results for sample AD29790, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29790.D Vial: 24 Acq On : 16 Dec 2001 12:56 am Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.51 ug/1 850597 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Butane,/2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 1,3-Dioxolane, 2- (3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 278 (7.599 min): 29790.D (-) m/ z 73.00 100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 8.00 36 1, 1 50 55 xdddnn/mT1. 67, i — m/z 4 3.00 28.90% ■ ■ । ——————— miz->10 20 30 40 50 60 70 80 90 100 110 'Abundance #62932: Silane, tetramethyl- 73

5000- 7.20 7.40 7.60 7.80 8.00 45 m/z 4 5.0.5 11.19% 15 53 59 88 — । —I Opd—u*ifm m/Z-> 10 20 30-40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 3.0 73

710 1 i 1 ■ 7.20 7.40 7.60 7.80 8.00 5000- m/z 44 58 15 ' ' i ■ ' ' । ■ * 1 ■ । ■ ■ • ■ । ■ I . । T , 1 -I-1-1-1-!->" | | ' l m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- ' 1 1 1 ■ 1 1 TITTTumr 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 6.26% 5000 55 ■ 87 27 33 45 > ■ i ■ • ■ • i ■ > • • i ■ ■ ■ ■ i > 1 ■ ■ । TInTT । । ■ ■ I ’ 1 ■ ■ । ■ ■ 1 ■ । ■ ■ ' 1 i 1 1 1 1 i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29790.D GCMS1126.M Fri Dec 28 13:25:49 2001 . Page 1

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