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GC/MS analysis report, sample AD23720, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23720 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089218–000089233

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089231
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23720.D Vial: 16 Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS Sample : g'c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Propanedioic acid, hexyl-, die Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 35.66 0.63 ug/1 56220 Perylene-dl2 37.23 Hit# Of 5 ritative ID MW MolForm CAS# Qua! 1 Propanediplc acid, hexyl-, diethyl 244 C13H24O4 005398-10-7 27 2 2,4,6 (1I0H, 5H) -Pyrimidinetrione , 5 240 C12H20N2O3 051209-93-9 17 3 Methyl /4-nitrophenyl sulphoxide 185 C7H7NO3S 000940-12-5 16- 4 1-Dec^e, 2,4-dimethyl-_____________ 168 C12H24 055170-80-4 12 Abundance Scan 3335 (35,660 min): 23720,0 (-) m/z 185.10 100.00% Ite

57 5000 70 43

JhUILjLXt. 208' TT-r-p-t-r 281 m/z T 35,40 35,60 35.80 36,00 57.00 152 .42% Tife-> 20 40 60 80 100 120 140 160 180 200 :220 240 260 280 Abundance #32687; Propanedioic acid, hexyl-, diethyl ester 57 70

253 83 112 A 35,40 35,60 35,80 36,00 m/z TOTOO"^ 40.27% 199 217 ■I''''I''''I'' ' 'I ' ' ' ' I ' ‘ ' I '''' I'' ' ' I'' '' I' ' nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #31909:2,4,6{1H,3H,5H)-Pyrimidinetrione, 5,5-diethyl-1-(1- ------- ----- ---- ——1$5—-- —---- A 35,40 35,60 35,80 36,00 5000 Wz 71.00 39711% 211 54 96 -- —- — I-- ' ' ’ p ' r I . I I I I I I I I ] k . I I I I I I . I :j7- .•1.^2^., -197- -- TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 '\bundance #19102: Methyl 4-nitrophenyl sulphoxide _________ _ _ Ite,____ 35,40 35,60 35,80- 36,00:— =m/z*- 43-. 05 -28t79%

253 170 -30- 92 A A ’+*7 ...................... Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 35,40 35,60 35,80 36,00

23720.D NP091101.M Tue Oct 16 15:15:55 2001 Page .6 ■

NYC-WTC_000089231

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NYC-WTC_000089231Source: NYC Law Department, mirrored locally

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