NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1501\23720.D Vial: 16
Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS
Sample : g'c/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library ; C:\DATABASE\NBS75K.L
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Peak Number 6 Propanedioic acid, hexyl-, die Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
35.66 0.63 ug/1 56220 Perylene-dl2 37.23
Hit# Of 5 ritative ID MW MolForm CAS# Qua!
1 Propanediplc acid, hexyl-, diethyl 244 C13H24O4 005398-10-7 27
2 2,4,6 (1I0H, 5H) -Pyrimidinetrione , 5 240 C12H20N2O3 051209-93-9 17
3 Methyl /4-nitrophenyl sulphoxide 185 C7H7NO3S 000940-12-5 16-
4 1-Dec^e, 2,4-dimethyl-_____________ 168 C12H24 055170-80-4 12
Abundance Scan 3335 (35,660 min): 23720,0 (-) m/z 185.10 100.00%
Ite
57
5000 70
43
JhUILjLXt. 208'
TT-r-p-t-r
281
m/z
T
35,40 35,60 35.80 36,00
57.00 152 .42%
Tife-> 20 40 60 80 100 120 140 160 180 200 :220 240 260 280
Abundance #32687; Propanedioic acid, hexyl-, diethyl ester
57
70
253
83 112
A
35,40 35,60 35,80 36,00
m/z TOTOO"^ 40.27%
199 217
■I''''I''''I'' ' 'I ' ' ' ' I ' ‘ ' I '''' I'' ' ' I'' '' I' '
nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #31909:2,4,6{1H,3H,5H)-Pyrimidinetrione, 5,5-diethyl-1-(1-
------- ----- ---- ——1$5—-- —----
A
35,40 35,60 35,80 36,00
5000 Wz 71.00 39711%
211
54
96
-- —- — I-- ' ' ’ p ' r I . I I I I I I I I ] k . I I I I I I . I
:j7- .•1.^2^.,
-197- --
TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
'\bundance #19102: Methyl 4-nitrophenyl sulphoxide
_________ _ _ Ite,____ 35,40 35,60 35,80- 36,00:—
=m/z*- 43-. 05 -28t79%
253 170
-30-
92 A A
’+*7 ......................
Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 35,40 35,60 35,80 36,00
23720.D NP091101.M Tue Oct 16 15:15:55 2001 Page .6 ■
NYC-WTC_000089231
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