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GC/MS analysis report, sample AD23720, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23720 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089218–000089233

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089230
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23720.D Vial: 16 Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************* * * * * * * * * **************** Peak Number 5 D-Limonene Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 12.12 0.92 ug/1 86412 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

D - L imonene 136 C10Hi6 005989-27-5 94 Limonene 136 C10H16 000138-86-3 90 3 Cyclohexene, l-methyl-4-(1-methylet 136 C10H16 007705-14-8 90 4 Cyclohexene, 1-methyl-4-(1-methylet 136 C10H16 005989-54-8 72 Msundance Scan 771 (12.122 min); 23720.D (-) m/z 68.00 100.00% 6|3 93 5000 79 39 53 107 121 136 T

20 30 40 50 60 70 80 90 100 '... .... 110 A 120 130 140 11.80 12.00 12.20 12.40 m/z66.95 69.14% Abundance #65790; D-Limonene 6|3

93 5000 I”' ' ' ' I ' ' ' ' ' I ' ' ' ' I . 11.80 12.00 12.20 12.40 53 79 107 121 136 "m7^ 97700 66723%

n/z-> 20 30 40 I • I * ' ' '~l ' ' ' ' I ' 50 60 70 4 80 90 100 ,.l.. T ,, 110 120 130 140 Abundance #65774; Limonene gb-------- ---- -------- -

.11.80 12.00 12.20 12.40 5000 93 79705 30.20% 27 53 79 107 121 136 -1^ ’iji.TT." ~l Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140. Abundance #6633; Cyclohexene. 1-methyl-4-{1-methylethenyl)-, (.+/-.)- _____ _____ 6b---- t^11-.80-12;00-12;20-12.-40— - -m/z — 947-00----- 25T49%

553 93

• I ■ ■ ■ ■ I ■ ' • > 1 > ■ > > I ' ' ' • I ' • I 79 i|.. T. ' I ' ' ' ' I ' r I’l I . ■ I I I 1 I I . I I I I I I ■ I I 20 30 40 50 60 70 80 90 100 110 120. 130 140 11.80 12.00 12.20 12.40

23720.D NP091101.M Tue Oct 16 15:15:53 2001. Page 5

NYC-WTC_000089230

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NYC-WTC_000089230Source: NYC Law Department, mirrored locally

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