NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1501\23720.D Vial: 16
Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
********************************************* * * * * * * * * ****************
Peak Number 5 D-Limonene Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
12.12 0.92 ug/1 86412 1,4-Dichlorobenzene-d4 11.76
Hit# of 5 Tentative ID MW MolForm CAS# Qua!
D - L imonene 136 C10Hi6 005989-27-5 94
Limonene 136 C10H16 000138-86-3 90
3 Cyclohexene, l-methyl-4-(1-methylet 136 C10H16 007705-14-8 90
4 Cyclohexene, 1-methyl-4-(1-methylet 136 C10H16 005989-54-8 72
Msundance Scan 771 (12.122 min); 23720.D (-) m/z 68.00 100.00%
6|3
93
5000
79
39 53 107 121 136 T
20 30 40 50 60 70 80 90 100
'... ....
110
A 120 130 140
11.80 12.00 12.20 12.40
m/z66.95 69.14%
Abundance #65790; D-Limonene
6|3
93
5000 I”' ' ' ' I ' ' ' ' ' I ' ' ' ' I
. 11.80 12.00 12.20 12.40
53 79
107 121 136
"m7^ 97700 66723%
n/z-> 20 30 40
I
• I * ' ' '~l ' ' ' ' I '
50 60 70
4
80 90 100
,.l.. T ,,
110 120 130 140
Abundance #65774; Limonene
gb-------- ---- -------- -
.11.80 12.00 12.20 12.40
5000 93 79705 30.20%
27 53 79 107 121 136
-1^ ’iji.TT." ~l
Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140.
Abundance #6633; Cyclohexene. 1-methyl-4-{1-methylethenyl)-, (.+/-.)-
_____ _____ 6b---- t^11-.80-12;00-12;20-12.-40— -
-m/z — 947-00----- 25T49%
553 93
• I ■ ■ ■ ■ I ■ ' • > 1 > ■ > > I ' ' ' • I ' • I
79
i|.. T.
' I ' ' ' ' I ' r I’l I . ■ I I I 1 I I . I I I I I I ■ I I
20 30 40 50 60 70 80 90 100 110 120. 130 140 11.80 12.00 12.20 12.40
23720.D NP091101.M Tue Oct 16 15:15:53 2001. Page 5
NYC-WTC_000089230
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