Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
NYC-WTC_000036469–000036479Folder label: “GCMS X 12/5/01 A 12/12/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C : \HPCHEM\ 1 \DATA\DEC12 0 1\29461.D Vial: 18 Acq On 12 Dec 2001 7:35 pm Operator: 209 GALOS Sample gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
7.60 3.60 ug/1 1034900 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-Ethylform ide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxol e, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 Silane, t ramethyl- 88 C4H12Si 000075-76-3 9 4 1,3 -Diox ane, 2-methyl- 88 C4H802 000497-26-7 5 Abundance Scan 278 (7.600 min): 29461.0 (-) m/z 73.00 100.00% 7b
5000- 43 7.20 7.40 7.60 7.80 8.00 37, |, | 49 55 67, । |......... 87 ............ 103.................... ■ • I ■ ■ ■ ' I > ■ l ■ ■ > । । i i . . । . TTTt 1 m/z 43.00 26.74% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73
5000 7.20 7.40 7.60 7.80 8.00 44 58 m/z 44.95 9.89% 154 ' TH • ( • ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 TIT—merrmrrtur 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 8.87% 45 36 55 67 ......................1.09,1,1,5, ' 1 1 1 1 1 1 i ' ■ ' ■ i ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #845: Silane, tetramethyl- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.53% 5000-
45 15 31 | 55 1 88 > > i > > ■ > i ■ ■ 1 1 l'1 1 1 1 I 1 1 1 1 1 1 YIT । । । । । । 1 ■ ' i ■ • ' ' i ■ ' ' ■ i 1 ' ' ' 1 1 1 ' 1 1 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 3.00
29461.D GCMS1126.M Fri Dec 21 12:28:39 2001 Page 1
NYC-WTC_000036476
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NYC-WTC_000036425
Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036360
Laboratory GCMS analysis report for sample AD29289 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036403
Laboratory report documenting GCMS analysis of sample AD29299 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036337
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036338
Laboratory report showing GCMS analysis results for sample AD29289 with surrogate and unknown compound data.
Filed in the same folder
NYC-WTC_000036341
Calibration log for GCMS analysis of sample AD29289 listing target analytes and detection limits.
Filed in the same folder
NYC-WTC_000036345
Reference standard analysis report for GCMS testing showing concentrations of target analytes and detection limits.
Filed in the same folder
NYC-WTC_000036350
Blank sample analysis report for GCMS testing showing non-detect levels for target analytes.
Filed in the same folder