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Document / 13 pages

GCMS analysis results for sample AE00008, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00008 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050109–000050121

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050120
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\8.D Vial: 10 Acq On : 24 Jan 2002 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHCDS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzoic acid, 2-[(trimethylsil Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.13 1.17 ug/1 • 407021 Naphthalene-d8 15.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic Acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 47 2 Benzeneethanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 47 3 Cyclo; ntasiloxane, decamethyl- 370 C10H30C5Si5 000541-02-6 .42 4 11H-D ibenzo[b,E] [1,4]diazepin-11-on 267 C16H17N30 013450-73-2 30 Abundance ‘ Scan 990 (14.134 min): 8.D (-) m/ z 73.00 100.00% 73

5000- 267 355

45 13.80 14.00 14.20 14.40 1 I ! 103118133 154 177 193208223 251 293 IwuuOTmTuuuuTTuuur 323 339 I I ■'1 ■ i' ■ ° i' ■ ■ '11 m/z 267.0.0 38.19% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi 73 267

.................. ....... 5000 13.80 14.00 14.20 14.40

135 m/z 355.0,5 29.74% 47 175 193209 233 249 WIIUTr J t i ■1' ■ r ' ■' i • ■ ■ ■ i ■ * । . . utvvonni . । । J 282 ' i' ■'' i ■ ■1 ■ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-Atpentafluorophenyl)methylene] 73 T T 13.80 14.00 14.20 14.40 5000- m/z 356.05 10.26% 267 44 151 179194209 250 ■■। ।■ ’’’’I’" ." I TVPu—mmanTTT TTTTT l’ ’ ’I’’’’ ].... I.... I m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 'Abundance #51266: Cyclopentasiloxane, decamethyl- / \ 73 13.80 14.00 14.20 14.40 m/z 267.90 10.19% 355 267 5000-

1 191207 251 323 339 TTpTT-rpnTTTTTTTpnn-TpT-rrpTnTyTTTTpnrn-rpnn^ TTIT I’ ’" I i... I.... I ... - m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40

8.D GCMS0208.M Fri Feb 08 13:43:15 2002 Page 5

NYC-WTC_000050120

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NYC-WTC_000050120Source: NYC Law Department, mirrored locally

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