GCMS analysis results for sample AE06449, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR17O2\6449 .D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.10 2.95 ug/1 382656 1,4-Dichlorobenzene-d4 12.21

Tentative ID MW MolForm CAS# Qual ----- 5 7r---- Hit# of 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Dioxglane, 2-pentadecyl-_____ 284 C18H3602 004360-57-0 9 Abundance ’ Scan 332 (8.096 min): 6449. D (-) m/ z 73.00 100.00% 73

5000 43 _____ / 1 1 1 I ‘ 1 ' ,-l ' 1 ' ' I ' • ‘ ' I 1 1 ' ' 7.80 8.00 8.20 8.40 37, 1149 55 . 87 103 ■ i ' 1 ■ 1 I1 ' ' 1 i 1 ' ' ' i ' 67 I m/z 43.05 27.62% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73

5000 1 * Ti”* ■ r । 1 1 T • i ■ ■ 11 i 1 ' ■ * 7.80 8.00 8.20 8.40 m/z 41.05 10.72% 45 15 | 53 59 - T TH — — 88 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 —— T — — A ,.r 7.80 8.00 8.20 8.40 5000 m/z 45.05 9.64% 44 58

15

m/z-> - - 4—— 1G 20 301 1,11 l — 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet __________ ___________ ■ r 1 । 1 1 1 1 । 1 1 1 1 । 1 ■ ■ 1 । r ■ ■ ■ 73 7.80 8.00 8.20 8.40 m/z 71.00 6.81% 5000

45

m/z-> -----% L 10 20 30 40 55 60 67 1 1 i ■ ‘ 1 ' i 1 1 1 1 i 1 50 70 - 80 90 100 109115 ■ i ‘ ' 1 ' i ‘ 1 110 120 7.80 3.00 8.20 8.40

6449.D GCMS0412.M Thu Apr 18 09:10:43 2002 Page 1

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