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GCMS reference data for sample AE05847, April 16 2002

Machine-extracted title · confidence 90%

Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.

NYC-WTC_000059608–000059618

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO4 O2\5847.D Vial: 21 Acq On 4 Apr 2002 5:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Carbon dioxide Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 7.76 0.63 ug/1 29289 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Carbon d^xide 44 CO2 000124-38-9 4 2 Ethylene'’ oxide 44 C2H4O 000075-21-8 3 3 Acetaldehyde 44 C2H4O 000075-07-0 3 4 Ethyne,/ fluoro-__________________ 44 C2HF 002713-09-9 3 Abundance / Scan 296 (7.761 min): 5847.D (-) mTz 39795 100.00% 40

44 253

740 7.60 7.80 8,00 8.20 36 42 46 51 mTz 43790 51.83% I ' ' ' ‘ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ' ' P ’ I ' ' ' ' I ' ' ' ' I ' ' ' ' I Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 Abundance #62263: Carbon dioxide 44

5000 - i-rp I - -I I I I I Ppp. r i-i-i 7 40 7.60 7.80 8,00 8.20 m/z 3^790 1.12% . ?, 5 10 15 20 25 .. ..30 35 40 45 46 50 55 60 Abundance #62267: Ethylene oxide 20 44

15 7 40 7.60' 7.80 8.00 8.20 253 in/z 44.95 0.91%

42

m/z-> ......... 5 10 13 I INI '^-1— ill. 31 15 20 25 30 26 35 .mi* 40 45 ' I ' ' ' ' I ' ' ' ' I 50 55 60 Abundance #36: Acetaldehyde / 2|9 740 7.60 7.80 8.00 8.20 44 m/z 42.05 0.61% 5000

rn/z-> 5 10 15 20 25 31 ' I ' ' 30 35 40 42 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 45 50 55 60 7,40 7.60 7.80 8.00 L 8^

5847.D GCMS0408.M Tue Apr 16 08:17:08 2002 Page 1

NYC-WTC_000059615

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NYC-WTC_000059615Source: NYC Law Department, mirrored locally

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