GCMS analysis results, sample AE08761, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8761.D Vial: 23 Acq On : 23 Apr 2002 6:35 am Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethanone, 2-bromo-l-phenyl - Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

33.35 0.29 ug/1 38742 Chrysene-dl2 33.64

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanone, 27bromo -1 -phenyl - 198 C8H7BrO 000070-11-1 17 2 Benzoic acid, ethyl ester 150 C9H10O2 000093-89-0 17 3 1,2 -Bis (benzoyloxy) benzene 318 C20H14O4 000643-94-7 12 4 Ethanone, 2-(formyloxy)-1-phenyl- 164 C9H8O3 055153-12-3 12 Abundance Scan 3083 (33.348 min): 8761 .D (-) m/z 104.95 100.00% 105 149 ___

5000 77

51 163 33.00 33.20 33.40 33.60 11111 fftTTPm 111 ii 111।।।।।j।।11 TTT m/z 149.00 90.36% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #69582: Ethanone, 2-bromo-1-phenyl- 105

/ 5000 ■ ■ i ■ • ■ ■ i i’ 77 33.00 33.20 33.40 33.60 m/ Z 77.05 47.32% 51 --91 ! 111 ■ ■ ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ ■' i 200 ■11 ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i • ■ ■ ■ i ■ ■ ■ ■ i mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320

L Abundance #66754: Benzoic acid, ethyl ester 105 AL 33.00 33.20 33.40 33.60 5000 77 m/z 162.95 13.64% 122 150

mz-> 20 40 L 51

60 । ‘ 91 । ■ * rn ■ * *"* i1 * • ■ । ■ ■' ■ । ■' ■ ■ । * * ■ ■ । 80 100 120 140 160 180 200 220 240 260 280 300 320 * i ‘ *1' ।111 ■ । ■111 ■ ■'11 *1

Abundance #45379:1,2-Bis(benzoyloxy)benzene TIiB 105 33.00 33.20 33.40 33.60 m/z 51.00 12.40%

5000 77 M 27 51 111 " i111 r i1 121 137 197 213 318 mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 33.00 33.20 33.40 33.60

8761.D GCMS0412.M Tue Apr 23 14:23:56 2002 Page 3

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