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Document / 9 pages

GCMS blank analysis results, April 2002

Machine-extracted title · confidence 90%

Instrument calibration record using DFTPP standard to verify GCMS performance for analytical testing on April 1, 2002.

NYC-WTC_000059478–000059486

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059485
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRO102\LBA.D Vial: 16 Acq On : 2 Apr 2002 3:07 am Operator: Sample : gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Propanone, 2,2-dichloro-3-hy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.41 0.40 ug/1 45718 Chrysene-dl2 33.69

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propan/ne, 2,2-dichloro-3-hydroxy 218 C9H8C12O2 054824-08-7 12 2 Ethaned/bne, diphenyl- 210 C14H10O2 000134-81-6 12 3 EthanoD^, 2-chloro-l-phenyl- 154 C8H7C1O 000532-27-4 12 4 2-Bro^^isobutyrophenone 226 ClOHllBrO 010409-54-8 12 Abundance" “ ‘ ....... .. ............ Scan 3089 (33407 minj; lba^D H m/z 104?^. 1(15 149

i 5000

51, 77

163 a/V . .. . 33.00 33.20 33.40 33.60 33.80 .............. I.......I,....... ........ ........ ............................................................ . ............. ................. m/z 149.00 92.00% __ :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200 210 'Abundance #27040: 1-Propanone, 2,2-dichioro-3-hydroxy-1-phenyl- I 1(1)5 i

5000 77 33.00 33.20 33.40 33.60 33.80

51 i ...30 63 89 .7-.................... ... ........... 166... 188....... 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170180 190 200 210 'Abundance #70131 Ethanedione diotisnyl- 165

33.00 33.20 33.40 33.60 33.80 5000 77 m/z 51.00 11.57% ! i 51. i 27 39 151 210 'm/z-> :20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210__ Abundancei #67044: Ethanone. 2-chloro-1-phenyl- 1(1)5 33.00 33.20 33.40 33.60 33.80 m/z 163.05 9.86% 5000 77

51 I X a. "nr 154 • I ‘‘ I"'' r "' I n m/z-> 20 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 210 33.00 33.20 33.40 33,60 33.80

LBA.D GCMS0403.M Fri Apr 05 10:42:03 2002 Page 2

NYC-WTC_000059485

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NYC-WTC_000059485Source: NYC Law Department, mirrored locally

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