GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31504.D Vial: 12 Acq On : 19 Jan 2002 2:21 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.68 ug/1 165232 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone,/ 1,1,1-trichloro- 160 C3H3C130 000918-00-3 25 2 4-Penten-2-one 84 C5H80 013891-87-7 12 3 1-Acetoxy-2- (dodecyloxy) ethane 272 C16H32O3 000000-00-0 10 4 Ethanone/ l-cyclopropyl- 84 C5H80 000765-43-5 9 Abundance Scan 277 (7.585 min): 31504.D (-) m/ z 43.05 100.00% 43

5000 i f-r i ri j-'i i ( i । . 1it7) । i । 1 । i i 82 97 125 7.20 7.40 7.60 7.80 8.00 , . , 63 „ I, ' — viaei 100 I. 120 UP 160 180 200 220 240 260 ‘ m/z 124.95 9.84% m/z~> 20 40 60 80 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 । j > > > > । ■ । 7.20 7.40 7.60 7.80 8.00 15 m/z 81.85 7.45% I.. , . 85 97 125 ■ ■ i ■ ■ ■ ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #555:4-Penten-2-ore 43

7.20 7.40 7.60 7.80 8.00 5000 m/z 96.95 7.21% 15 27 69 84 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #38130: 1-Acetoxy-2-(dodecyloxy)ethane ■ i 1 ■ ■ ■ i 1 ‘ ‘ ■i • ‘ ‘ ' i ‘ ■ ■ i ■ ■ 4(3 7.20 7.40 7.60 7.80 8.00 m/z 82.85 7.06% 57 5000 71 87

| • ■ । * i । > ■ i I ll 29 111 197 212 272' i i ■ • ■ • i11 ■11 • 1 ‘ ' 111 ■ ‘ i 1 ' ■ ‘ 11 ' 1 ■ i ' ‘ • '■ i ‘1 11 i ■ ■ ■ ' i ■ ■ ■ ■ i ■ ‘ ‘ I ! ‘ ‘ ' I ' ‘ ' I ' ‘ ‘ ' I ‘ Ckid l 1 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 7.20 7.40 7.60 7.80 8.00

31504.D GCMS0103.M Wed Feb 06 15:38:28 2002 Page 2 NYC-WTC_000016633