GCMS sample AE07770 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07770 including detection of unknown compounds.

NYC-WTC_000049008–000049026

Folder label: “GCMS X 4/12/02 A 4/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR2202\7770.D Vial: 19 Acq On : 23 Apr 2002 2:43 am Operator: Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 .beta.-D-Ribofuranose, 1-aceta Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

33.35 0.27 ug/1 57610 Chrysene-dl2 33.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 .beta.-D-Ribofuranose, 1-acetate 2, 504 C28H2409 006974-32-9 16 2 1-Benzoyloxy-2 -formyloxybenzene 242 C14H10O4 797922-93-1 12 3 Ethanone, 2-bromo-1,2-diphenyl- 274 C14HllBrO 001484-50-0 12 4 Benzoic acid, henyl ester 198 C13H10O2 000093-99-2 12 Abundance Scan 3083 (33.352 min): 7770.D (-) m/z 104.90 100.00%) 1(6 149

5000 77

51 163 33.00 33.20 33.40 33.60

mz-> 40 Lu * 11 *•■!••••।■■* *।...*11... ।।।।।।। 60 1 80 100 120 140 160 180 200 220 240 260 280 300 320 207 281 Toi . . 1 . |T-r m/z 149.00 82.21% Abundance #59067: beta.-D-Ribofuranose, 1-acetate 2,3,5-tribenzoate 105

5000 77 33'ob 33.20 33.40 33.60 m/z 77.05 39.92% 51 122 TT I ‘ ‘ 201 322 * I ‘ ' I 1 UIT I i i i । i m i p » ‘ ' P ' ‘ ‘ I ‘ ‘ ‘ ‘ I ‘ ‘ t ri i । i i i » । : i ITT miz-> 40 00 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32316:1-Benzoyloxy-2-foimyIoxybenzene 105 —Al 33.00 33.20 33.40 33.60

M) 5000 77 m/z 51.00 9.95%

51 11 > 11 "T* *t । 197 214 242 i • •।• i •' ■■i ■11 ■ i ■ • ••i■ ■ • ■ i • ■ • •i‘■ i ■ ■ ‘ ■ i■■1 ■ i •1 ■ • i ••■■ i ■ ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #38426: Ethanone, 2-bromo-1,2-diphenyl- ‘ J * ‘ TF 105 33.00 33.20 33.40 33.60 m/z 162.95 9.25% 5000

A 77 51 91 165 196 —pL 11)4 ■ ■ ■ 11 mfe-> 40 60 80 100 120 140 160 180 200 220‘ 240 260 280' ‘360' 320 33.00 33.20 33.40 33.60

7770.D GCMS0412.M Tue Apr 23 14:23:24 2002 Page 3

NYC-WTC_000049025

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NYC-WTC_000049025Source: NYC Law Department, mirrored locally

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