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GCMS analytical results for sample AE03831, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03831 analyzed on March 29, 2002.

NYC-WTC_000038084–000038092

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Library Search Compound Report

f Data File : C:\HPCHEM\1\DATA\MAR2202\3831.D . Vial: 12 Acq On : 23 Mar 2002 4:56 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.97 ug/1 140945 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopenta loxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N- (Triflu oacetyl)-N,O,O' ,0''-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 Phenethy mine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzoic- j cid; 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance 73 Scan 1069 (14.863 min): 3831.D (-) m/z 73:00 100.00%

5000 267 355 — r 4— 45 119 154 193 223 , ____ 14,60 14.80 15.00 15.20 : —— 323 I-T nr 1-- TITTT m/z 267.00 43.31% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl-' 73 355 267 । - -i--i-1 — — 5000 14.60 14.80 15.00 15.20 m/z 355.05 42.67% ............................. 207 . | 323. I miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N O.O’,O"-tetrakis(trimefhylsi 73 ■ ■ i ■ ■ • ■ । __ ' • i 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 14.73%

45 147 193 267 I 538 1 1 1 ' m/z-> 50 100 150 200 250 300 400 350 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 14.60 14.80 15.00 15.20 m/z 268.00 11.71% 5000 355 44 1 147 193 267 294 i ' ' ' ' i ‘miz-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

3831.D GCMS0308.M Tue Mar 26 14:59:32 2002 Page 1

NYC-WTC_000038091

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