GCMS analysis results for sample AE02575, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Pentane, 3-methoxy- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

8.15 0.48 ug/1 70625 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 L Tentative ID MW MolForm CAS# Qual

1 Pentane, -methoxy- 102 C6H140 036839-67-5 28 2 N-Ethylformamide 73 C3H7N0 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3-Dioxolane, 2 -(3-bromo-5, ,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 338 (8.152 min)/2575.D (-)'■ , m/z 73.00 100.00% 73

5000 43 TETET/TII 1 1 ' 1 | 1 1 । r । । i < । [ i 7.80 8.00 8.20 8.40______ - 149 55,....... _L ■ ' 10— 1 1 ' 'T1 87 103 m/z 43.05 ~ 3 0.3 0% miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73

m/z-> 5000-

Abundance ......... 2733 39_ 10 20 30

30 40 45

1 1 [

50 1 55 1 ' ! ' |

60 ' l ) ' |

70 ,

73 I > > |

80 > I I I |

90 I 1 ! I

100 | ! I I I

110 | I ’ 1 1 1 1 7.80 m/ z 41 ' ° 8.00

— ■ i 1 1 1 1 i 8.20 ■1 1 ’ i * 8.40_______ 11.15%

A A 1 1 1 ' 1 ' 1 1 A—M— 7.80 8.00 8.20 8.40 ______ 5000- m/ z 45.05 9.26% 44 58

15 1 ■ l ■ ■ ■ ■ | ' 1 ■ ■ ) 1 ■ ■ 1 | ■ > > > I 1 • ■ i I > > > > I i r r ■■| | i i | I 1 1 > > | 1 1 1 1 [ > m/z-> ....... 10 20 30 40 50 60 70 80 90 100 110 — Abundance #845: Silane, tetramethyl- 73 7.80 8.00 8.20 8.40 ____ m/z 71.00 7.48% 5000

, 45

m/z-> 5......31 55 1 1 1 1 1'111 1 1 1 1 1 1 88 1 ' I 1 1 1 ' I 1 1 1 1 1 1 ' 1 1 1 ‘ 1 । ' 1 n 1 1 1 i 1 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

2575.D GCMS0308.M Thu Mar 21 14:23:22 2002 Page 1

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