GCMS analysis results, sample AE05231, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5231.D Vial: 42 Acq On : 31 Mar 2002 9:38 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L V

Peak Number 1 Pentane, 3-methoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.13 0.48 ug/1 55996 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane,/3-methoxy- 102 C6H14O 036839-67-5 9 2 Silane, /tetramethyl - 88 C4H12Si 000075-76-3 9 3 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 4 1-Butanamine, 3-methyl- 87 C5H13N __ 000107-85-7 7 Abundance / “ ' ......Scan 33618^33 min): 5231 .D (-) m/ z 73.00 100.00% i I 7l3

5000 43 ___ 55 87 103 7.80 8.00 8.20 8.40_____ I ' ‘ ' I 4- m/z 43.05 32.67% Uz-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #1793: Peritane, 3-methoxy- I 7)3

... . 5000 45 7.80 8.00 8.20 8.40 m/z 45.05 12.10% y 33 39| 55 ''' ' I-' ■'■•'•I ' ....................... ... , ......................................... fn/z-> ' 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silar.e. tetrameitiy'- I I I I I I r I 1?^ T __ 7.80 8.00 8.20 8.40 5000 m/z , 41.05 11.22% i iI 15 31 45 55 88 ni/z-> 10 20 30 40 50 60 70 _'_80 90 100 110 'Abundance #63573: 3-Pentanol. 3-me'thyl- 7|3 7.80 8.00 8.20 8.40 m/z 71.00 6.51% A 5000

55 45 I 87 27 I , 39, I I. m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5231.D GCMS0308.M Wed Apr 03 13:55:39 2002 Page 1

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