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GCMS unknown compound analysis, sample AE05700, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.

NYC-WTC_000059248–000059257

Folder label: “GCMS X 3/11/02 A 4/1/02

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Scanned page image, NYC-WTC_000059255
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0102\5700.D Vial: 15 Acq On 2 Apr 2002 2:08 am Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Pentane, 3-methoxy­ Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 2.66 ug/1 375761 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane/ 3-methoxy- 102 C6H14O 036839-67-5 25 2 N-Ethy^ormamide 73 C3H7NO 000627-45-2 9 3 Silan^ tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3-d/0X0lane, 2-methyl- 88 C4H8O2 000497-26-7 7 Abundance Scan 336 (8.128 min): 5700.D (-) m/z 73 .’bo ’io'o.OO'% 7|3

5000- 43

3? I, I 50 55 67, I 87 103 __L80__81p_jB,20_8;4^^

L I..... . I m/z 43.05 28.75% m/z-->____ 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793; Pentane, 3-methoxy- 7)3

5000 . . I . I . 1 . I I • > |'i « . . I 45 7.80 8.00 8.20 8.40 m/z. 41.05 11.92% V 33 3?|. ' ' ’ I I 55 •'' ' I ' ' ■ I I I I ' ‘ ' I ' ' ' ' I ' ‘ ' I ' ' ' ' I ' m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-Ethylforrnaniide 30 73 7^0 8.00 8.20 8.40 5000 m/z 45.05 10.39% 44 58 ! .. ....I,.......... Tn/z--> JP___ 20 30 40 __50___ 6p_ 70___ 80___ 90__ 100 110 Abundance #845: Silane, tetramethyl- 7)3 7.80 8.00 8.20 8.40 m/z 71.00 6.99% 5000

45 ' I ' ' ' ' I I.... 88... ........ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5700.D GCMS0403.M Thu Apr 04 14:00:01 2002 Page .1

NYC-WTC_000059255

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NYC-WTC_000059255Source: NYC Law Department, mirrored locally

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