GCMS analysis report, sample AE04417, April 2002

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Data File : C:\HPCHEM\l\DATA\MAR2102\4417.D Vial: 8 Acq On : 21 Mar 2002 6:10 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Pentane, 3-methoxy- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 2.23 ug/1 317041 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentane, 3-methoxy- 102 C6H140 036839-67-5 25 2 1,3-Dioxola: , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 25 3 N-Ethylform imide 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-pentadecyl - 284 C18H36O2 004360-57-0 9 Abundance Scan 337 (8.142 mln): 4417.D (-) m/z 73.00 100.00% 73 5000 43 ' ■ I ‘ ‘ ‘ ■ I1 **I***-I‘***t 55 87 7.80 8.00 8.20 8.40 miz-> ■ ■ i ■ ‘ 10 ■ i ■ 20 — 30 374 40 A * 1*s""m ' 1 1 1 I1 + 50 60 70 80 t |

90 103 100 110 120 m/ z 43.05 28.91% Abundance #1793: Pentane, 3-methoxy- 73

5000 ' 1 I - II 45 7.80 8.00 8.20 8.40 m/ z 41.0,5 10.47% ‘ 27 33 39, 55 ■ ' 1 ' ' ' ' I ‘ ' I ‘ ‘ ' I 1 ■ ' ' I ' ‘ Cl I I J-t 111-B———n—n,—0mg miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49428: 1 3-Bioxclars, 203-promo-5.5 5-tricHior-2.2-dimet 73 rl • ’ ■ ' I 7.80 8.00 8.20 8.40 5000 m/z 45.05 9.72% 45 36 55 67 109 115 -*I**‘*I***-1‘4**1‘1I*‘I4**4I***I*41**II m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide .................. ) 30 m 1***1 7.80 8.00 8.20 8.40 73 m/z 71.00 7.32% 5000 44 58 15 P lkaaaaa 7.80' 8.00 - ‘1 miz-> 10 20 :30 40 50 60 70 80 90 100 110 120 8.20 8.40

4417.D GCMS0308.M Fri Mar 22 09:38:57 2002 Page 1

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