GCMS analysis results for sample AE07498, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1802\7498.D Vial: 6 Acq On : 19 Apr 2002 10:28 pm Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.11 0.34 ug/1 42107 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanbl, 3-methyl- 102 C6H140 000077-74-7 9 2 1,3-Dioxolane, 2 -(phenylmethyl)- 164 C10H12O2 000101-49-5 9 3 1,3 -Dioxolane 74 C3H602 000646-06-0 7 4 N-Ethylformamide_________________ 73 C3H7NO 000627-45-2 5 Abundance Scan 334 (8.114 min): 7498. D (-) m/ z 73.00 100.00% 73

5000 43 - 7.80 8.00 8.20 8.40 .......... 1,155..... ill i i।ni"। । । । । । । । i । i । । ।pi। । । । । I । । [ Ti 87 i i | i II 103 r | i i I i | i i i i । i i i i | i i i t | IUd) i ill | I ii I | i m/z 42.95 28.36% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 —A —I WA , ' i 7.80 8.00 8.20 8.40 55 m/ z 41.05 11.88%

m/z-> 20 275 30 40 50 .' r ...... ... ...... .1, 87 1 ■ ■ i ■ 1 ■ • i 1 ■ ■ ■ i ■ 60 70 80 90 100 110 120 130 140 150 160 170 YTT-rnq-rrn-TyT-T-r-rp-T-r-^^ n A

Abundance #13422:1,3-Dioxolane, 2-(phenylmethyl)- 73 A 7.80 8.00 8.20 8.40 5000 m/z 44.95 11.77% 91 45 65 103 120 ‘T‘‘"‘I‘11111TTTT-T‘TTTITTTT +t ' । ' 1 ■ ' i 1 1 ' ' । ''''' ■ । ' 1 1 ’ । ■ 1 1 ' । 1 ' ' 1 i ■ ’ ' ‘ । ' 1 ■ । । 164 1 1 1 1 । ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance 73 #320:1,3-Dioxolane 7.80 -4 8.00 8.20 ■ । ■ ■ ■ ' । 8.40 m/ z 71.00 8.82% 29 44 5000

....... . 1 1 1 ■ 1 'T' ' 1 ' 1 1 I’ m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 7.80 8.00 8.20 8.40

7498.D GCMS0419.M Mon Apr 22 10:43:20 2002 Page 1 NYC-WTC_000047015