GCMS calibration table for multiple compounds, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1202\LB.D Vial: 3 Acq On : 15 Apr 2002 10:03 am Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library. : C: \DATABASE\NBS7 5K. L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.70 ug/1 136007 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Benzoic acid, 2, 4-bis [ (trimethylsil 370 C16H3004Si3 010586-16-0 47 3 Phenethylamine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Noradrenaline, tetra-TMS_________ 457 C20H43NO3S14 000000-00-0 37 Abundance 7 Scan 1066 (14.828 min): LB.D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 t t l 108 133 154 177193 223 251 1.... ’’1’444114141 ‘ ,., (. t. 11।। n r । ■, r, । n .. j■.... । rif 111′4 ‘1+44 TIPTTPTTTT 323339 m/z 267.00 45.55% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 . ....... . 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 45.10% 191207 251 323339 I '' '4 I 4 ‘ 4 k H 4 4 4 I ’ * ’ 4 l ’ 4 4 4 1 4 4 4 4 I I ’ *'' l ‘ ‘4 * I i ■ ■ ■' i 1BBIpP9puuu27 i1444( miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 3(X) 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy}-, trimet 73 ............ ...........

14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.47% 45

133149 193 I 370 223 281 iz-> mospanumnipbampin 1!91001—110"0——100007 ‘ 2111/1111111111111T11111.‘E"T‘3331137-TT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyI-.beta.,3,4-tris(trimethyls 73 14.40 14.60 14.80 15.00 15.20 ' m/z 268.00 11.41% 5000 355

, 88 130147 193 267 294 — ■ i “' ‘ i “ ■ ‘ I ■ ■ ■ ■ i “ “ i ■" ■ i “ “ i ■1" i “'11' ■' ‘ i “ ■' i ■ “ ‘ i" I 1 1 1 1 I ■■ ‘ T T m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

LB.D GCMS0412.M Tue Apr 16 15:43:00 2002 Page 2 NYC-WTC_000048703