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Document / 22 pages

GC/MS calibration data for sample 30645, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018470–000018491

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018475
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.62 2.38 ug/1 977917 1,4-Diehlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 50 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pencane, 3-methoxy- 102 C6H140 _______ 036839-67-5 9 Abundance Scan 280 (7.616 min): 3O645.D(-) m/z 73.00 100.00% 73 5000 43 i • • ' ' i ■ > > ■ i * * • • i • * * • i • » 7.20 7.40 7.60 7.80 8.00 ,,,,,,,,,,,,,,, 38,1 ,1, 50,.55 +61.674 4r ■ ■ i ■ • ■ • i ■ ■ ■ • i ■ ■ ■ • I 1 1 ■ • I ■ ■ ‘ 87 103 ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' rn/z 43.00 32.70% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 " i'1' ■ t-H'i i i i . । i iFTTi i 7.20 7.40 7.60 7.80 8.00 45 m/z 45.0,5 11.64% 15 ‘ i ■ 1 • ■ i • ■ ■ 1 i ', । [ • i 53 • • I ‘ 59 । ''•’■ ■'i • • ■ ■ । । I ■ ■ । । 88 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 -mr rmmi ■ ■ ■ , IImm |' i f 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 11.50% 55 45 87 27 39, | 1 , 1 i ■ ■ • 1 i • : ' i ■ ■ ■ • i ■ • • • i • • ■ ■ i ' 1413 1 i ■ • ' • । ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide —TTTTFTTTTTIITITTTfrTt 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.98% 5000 44 58

15 miz—> 10 * 20 30 onnijapus 40 50 I ■ ' ' ■ I ‘ 60 70 IIIIIIIIIIIIIIIIIV

80 90 100 110 7.20 7.40 7.60' ' 7.808.00 '

30645.D GCMS1126.M Fri Feb 01 10:52:27 2002 Page 1

NYC-WTC_000018475

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NYC-WTC_000018475Source: NYC Law Department, mirrored locally

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