GCMS sample analysis AD29294, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29295.D Vial: 7 Acq On : 12 Dec 2001 5:35 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.03 ug/1 807394 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

.1 N-Ethylformami 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane/ 2-methyl- 88 C4H802 000497-26-7 9 3 1,3 -Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Thiocyanic acid, methyl ester 73 C2H3NS 000556-64-9 4 Abundance Scan 279 (7.603 min): 29295.D (-) m/ z 73.00 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00 37, |, | 49 55 .61 67, , |......... 87 ............ 103...................... ■|-| r1 1 । ‘I T’rn । । । TIT m/z 43.00 27.48% m/z-> 10 20___ 30 40 50 60 70 80 90 100 110 120 (Abundance #292: N-Ethylformamide 30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/ z 41.0.5 10.. 19%

m/z-> 10 —4 ' ■ i..... 20 30 40 50 । ■ ■ ■ ■ । ............... । । . ........ . , 60 70 80 90 100 110 120 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73 TT—Tm--ppeT 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 44.9,5 10.05% 58 27 | 87 . i ■ ■ ■ ■ i < • 1 i ■ • ■ ' i ' ' ' ' i ■ 1 ■ ' i ■ ■ ■ ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet “T । 4 . 1 . । . . . . । . . . TTPTTT , , | 73 7.20 7,40 7.60 7.80 8.00 m/z 71.0,0 5.74% 5000-

45 36 I | 55 67, 109 115 I ' . I I I . . i I I . — . | — T T-r-r-r T • ■ i ■ • • > i • ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29295.D GCMS1126.M Wed Dec 19 12:57:06 2001 Page 1

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