GCMS analysis results sample AD29298, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29298.D Vial: 25 Acq On : 13 Dec 2001 2:23 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 2.92 ug/1 784126 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3 -Dioxolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 5 4 Ethyl amine 45 C2H7N 000075-04-7 4 'Abundance Scan 279 (7.603 min): 29298.D (-) m/z. 73:00 100.00% 73

5000- 43 7.20 7.40 7.60 7.80 8.00 381 1___ 55 ’I' 67, 1 + ■ ■ i ■ ■ ■ 1 । ■ ■■■।■■■'r11'■i111 87 ■ ■ i ■ 103 m/ Z 43.05 26.40% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.95 10.52% 15 |.............. , miz-> 10 20 30 40 50 60 70 80 . 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-brorno-5,5.5-tricliloro-2,2-diinet 73 TI i . r i-|-i-Ti t । । I | iTi-l | 1-1

7.20 7.40 7.60 7.80 8.00 5000 m/ Z 41.00 9.88% 45 36 55 67 109 115 TIT . , । . , TIT . . . . । . I > . । . > > 1 ( . r-r-rT-r1-, m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62903: 1,3-Dioxolane, 2-methyl- TTTIPT TTuT 73 7.20 7.40 7.60 7.80 8.00 43 m/ z 71.00 6.83% 5000- 27 58 87 . — "ll — 1 1 1 1 1 i ■ ' > ■ i ■ 1 ■ ■ i ■ ■ ' ■ i ■ 1 ■ ■ i ■ ■ ' ■ । < • • > । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29298.D GCMS1126.M Fri Dec 21 12:20:51 2001 Page 1

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