Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
NYC-WTC_000036614–000036644Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 1-Butanol, 2,2-dimethyl- Concentration Rank 19
R.T. EstConc Area Relative to ISTD R.T.
7.48 3.35 ug/1 1401000 1,4-Dichlorobenzene-d4 11.53
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Butanol, 2, 2-dimethyl- 102 C6H140 001185-33-7 50 2 Acetic aci , isononyl ester 186 C11H2202 040379-24-6 43 3 1-Butanol, 2-ethyl- 102 C6H140 000097-95-0 38 4 2,4-Dim hyl-1-heptene 126 C9H18 019549-87-2 38 Abundance / Scan 265 (7.479 min): 29466.D (-) m/z 73.00 100.00% 73 43
5000 55 ' 1 I ' ' 1II ’ 1 TIp T I | . . . . 7.20 7.40 7.60 7.80 , 83, 95 103111 126 651 TTTTmp Tp-r । rr. i | . . . । । ।.. i. ।। । m/z 43.0.5 74.61% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #63536: 1-Butanol, 2,2-dimethyl- 43 71
5000- — I • 55 7.20 7.40 7.60 7.80 m/z 41.00 31.88% __ TI— 27 1 I 2111"1TTT" rn-p- TTT 87 ■ I11 " |1 ' r i yr. ■ . । . . . . । t i t ■ । I " ‘11 ‘ " • 11' " I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19454: Acetic acid, isononyl ester 43 57 T-r-j-r-r 7.20 7.40 7.60 7.80 70 5000 m/ Z 70.0.0 28.22% 27 115 83 I,...1,... ..... TIT I 1 1 i 126 186 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #63560: 1-Butanol, 2-ethyl- M TIImnnurr 43 7.20 7.40 7.60 7.80 m/z 55.00 24.02% 5000- 70 55 31 84 — I | ' r ■ " r ■ " i " ’' i ■'1 • i" 1 ‘I.... TEE I............................................. ‘I"TTTT‘‘EIICICITUITITTT‘TLETTCTTTTETTTT‘IIIITITII‘T Tr i l r. it । ( t-i-1 rrj । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 7.20 7.40 7.60 7.80
29466.D GCMS0103.M Wed Jan 09 16:16:02 2002 Page 1
NYC-WTC_000036624
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NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036492
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