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GCMS analysis results for sample AD29563, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036712–000036728

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036727
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L **************************************** ****** * * * * ** ** ** * * * * * * ******* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.25 0.44 ug/1 166574 Chrysene-dl2 33.02

Hit# of 5 Tentative 1 MW MolForm CAS# Qual 1 1 -Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 3-Isopropoxy-1,1/1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 4 2-Hexenedioi t acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 17 ■Abundance < Scan 2746 (30.250 min): 29563.D (-) m/ z 73.00 100.00% 73

5000- 147 221 ----------------- 281 355 I 45 17 117 191 249, .. 327, 401 1........................ 30.00 30.20 3G.40 30.60 ■ 'i1 ■ 1 ■ i ■ -AT m/z 147.00 38.56% m/z-> 50 100 150 200 250 300 .350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000- 147 ' 1 1 I 30.00 30.20 30.40 30.60 34 m/z 221.05 23.16%

m/z--> 50 103

100 l 150 200 250 — 281

300 — 325.. +42 350400 450 500 550 Abundance #60503: 3-lsopropoxy-1.1.1,7.7,r-hcxarnethyl-3,5,5-tris(trirn 73 / I 30.00 30.20 30.40 30.60 5000 m/z 355.05 15.55% 147

: T 2 327 415519561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 ■Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t i 73 30.00 30.20 30.40 30.60 m/z 281.00 15.15% 147 5000- 267 355 429 207

m/z-> • 45

50 100 150 —

200 250 ' ■ i ■ 300 L 350 400 450 500 550 I V,, j. , . I I 30.00 30.20 30.40 30.60

29563.D GCMS1126.M Tue Jan 08 11:42:43 2002 Page 9

NYC-WTC_000036727

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NYC-WTC_000036727Source: NYC Law Department, mirrored locally

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