GCMS calibration table with surrogate recovery data, Feb 16, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\FEB15O2\1137 .D Vial: 10 Acq On : 16 Feb 2002 12:12 am Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.29 ug/1 40257 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3 methyl - 102 C6H140 000077-74-7 36 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 36 3 3,4-Dimethyly5-hexen-3-ol 128 C8H160 000000-00-0 9 4 2-Butanone, B-methoxy-3-methyl- 116 C6H1202 036687-98-6 9 Abundance ......... / Scan 346 (8.217 min): 1137.D (-) m/ z 73.00 ‘ 100.00% 1 7)3

5000 43 i ■ ■ ■ ■ i 1 ' ' 1 i 1 1

m/z-> 111 ‘ 459+ ‘'1' I ■ ‘ 20 25i 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 , 8.00 8.20 8.40 8.60 m/z 43.0.5 87 41.22% 103 I j.।.. ।... > ।. i..।..., ।. i..।.. 1.1....।... 7.80

Abundance #63573: 3-Pentanol, 3-methyl- 73 ■

5000 1101 ■ ‘ I 1 ' 1 1 1 1 ‘ 7.80 8.00 8.20 8.40 8.60 55 m/z 45.05 14.62% 27 45 87 39 m/z-> mm Hmmmnpmp TT1n—unp2gmmamamm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance . ) < 6* lny! 73 - 7.80 8.00 8.20 8.40 8.60 5000 55 m/z 41.05 14.06% 87 27 45 33 j i > t.... I.... II.... I11Ijl!1111111111U11> rIJ11111riH11■11111111>11 m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #5018: 3,4-Dimethyl-5-hexen-3-ol AA i ■ ■ 1 ■ i * ' 1 1 I ‘ ‘ 73 7.80 8.00 8.20 8.40 8.60 m/z 39.0,5 10.14% 43 5000 55

27 | । , ,| 67,81 T’I—umnmmmptpWpgt 99 r/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.80 8.00 8.20 ‘ 8.40 8.60

1137.D GCMS0208.M Mon Mar 04 15:09:36 2002 Page 1

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