GCMS analysis results for sample AE02967, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB0 802\2967.D Vial: 31 Acq On 9 Feb 2002 2:28 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 2.47 ug/1 284090 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, -methyl- 102 C6H140 000077-74-7 28 2 1,3-Dioxola e. 2-methyl- 88 C4H802 000497-26-7 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane,3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 345 (8.213 min): 2967.D (-) m/ z 73.00 100.00% 73

5000 43

103 7.80 8.00 8.20 8.40 8.60 ................................ 38.1, .1 I50| I’5I,5'I , I . | 1 I 67 1 , 87 ' ‘ 1 ' 1 ' 1 1 1 1 1 1 1 1 ' 1 ' 1 I '| 'I ' ' ' i ■ ■ ................... .... • i ■ m/ Z 43.05 38.93% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.80 8.00 8.20 8.40 8.60 55 m/ z 45.05 13.19% 45 87 27 __________________ i 39, | -------- mz-> ■ ■ i 10 ' ■ ' ■ । ■ ■ ■ 20 ■ i ■ ■ 30 ■ 1 i ' ■ ■ ■ i ■ ' ■ ■ i ■ ' ■ ■ i ■ 40 50 60 70 80 90 100 110 Abundance 73 i 1 1 ■ ’ i ' ■ TPPmm 7.80 8.00 8.20 8.40 8.60 5000- 43 m/ z 41.05 13.00% 58 27 87 ——————————————— ' ' i ‘ ' ■ i ' ' ' ' i ' • ' ' i 1 1 1 1 I 1 1 1 1 1 1 1 ' ' 1 1 1 1 1 1 1 m/z—2 10 20 30 ... 40 50........ 60 _ 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyi- 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.57% 5000

15 41 55 70 87 T-r । i'i । । । । ' I-' ' ' 1′1 । ■ ■ i ' '' ' I 1 1 1 1 I ' 1 ' ‘ i ‘ i ' ' ' ' i ' ■ ' ■ i ■ ______ mlz—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

2967.D GCMS0208.M Wed Feb 13 11:08:36 2002 Page 1

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